Conformation analysis of d-glucaric acid in deuterium oxide by NMR based on its JHH and JCH coupling constants

d‐Glucaric acid (GA) is an aldaric acid and consists of an asymmetric acyclic sugar backbone with a carboxyl group positioned at either end of its structure (i.e., the C1 and C6 positions). The purpose of this study was to conduct a conformation analysis of flexible GA as a solution in deuterium oxi...

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Veröffentlicht in:	Magnetic resonance in chemistry 2016-07, Vol.54 (7), p.561-567
Hauptverfasser:	Enomoto-Rogers, Yukiko, Masaki, Hisaharu, Ito, Tetsuya, Furihata, Kazuo, Iwata, Tadahisa
Format:	Artikel
Sprache:	eng
Schlagworte:	carbon-proton coupling constant conformational analysis Deuterium Oxide - chemistry glucaric acid Glucaric Acid - chemistry Magnetic Resonance Spectroscopy Molecular Conformation NMR (J-resolved HMBC and NOESY) Thermodynamics
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