The Use of Optical Methods of Measurement to Investigate the Composition of New Aviation Materials

A procedure for the microwave sample preparation of nickel alloys to determine the mass fractions of Al, Ti, Cr, Co, Nb, Mo, Ru, Ta, W, and Re by atomic-emission spectrometry with an inductively coupled plasma is described. The compositions of the mixtures for solution and the parameters of the micr...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Veröffentlicht in:	Measurement techniques 2015-06, Vol.58 (3), p.362-366
Hauptverfasser:	Zagvozdkina, T. N., Karachevtsev, F. N., Dvoretskov, R. M., Mekhanik, E. A.
Format:	Artikel
Sprache:	eng
Schlagworte:	Accuracy Aeronautics Aluminum Analytical Chemistry Aviation Characterization and Evaluation of Materials Dispersions Error analysis Experiments Heat resisting alloys Inductively coupled plasma Investigations Laboratories Mass spectrometry Measurement Measurement Science and Instrumentation Measurement techniques Metals Methods Microwaves Nickel alloys Physical Chemistry Physics Physics and Astronomy Plasma Scientific imaging Spectrometry Statistical analysis
Online-Zugang:	Volltext
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	A procedure for the microwave sample preparation of nickel alloys to determine the mass fractions of Al, Ti, Cr, Co, Nb, Mo, Ru, Ta, W, and Re by atomic-emission spectrometry with an inductively coupled plasma is described. The compositions of the mixtures for solution and the parameters of the microwave dispersion are chosen. The limits of the relative error in measuring the mass fraction of the elements from 0.1% to 20% do not exceed 4% ( P = 0.95).
ISSN:	0543-1972 1573-8906
DOI:	10.1007/s11018-015-0717-z