Synthesis and physicochemical study of hexamminechromium(III) hexamolybdocobaltate

Synthesis and physicochemical study of hexamminechromium(III) hexamolybdocobaltate

Hexamminechromium(III) hexamolybdocobaltate [Cr(NH 3 ) 6 ][CoMo 6 O 18 (OH) 6 ] · 5H 2 O was prepared and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and powder X-ray diffraction. The crystals are monoclinic: a = 11.70 Å, b = 10.69 Å, c = 15.34 Å, β = 115.04°, V = 1905.11 Å 3 ,...

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Veröffentlicht in:Russian journal of inorganic chemistry 2013-07, Vol.58 (7), p.763-765
Hauptverfasser: Oreshkina, A. V., Kaziev, G. Z., Holguin Quinones, S., Milyutina, A. D.
Format: Artikel
Sprache:eng
Schlagworte:
Chemistry
Chemistry and Materials Science
Crystals
Diffraction
Infrared radiation
Inorganic Chemistry
Mass spectrometry
Spectroscopy
Synthesis
Synthesis and Properties of Inorganic Compounds
Thermogravimetry
X-rays
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Zusammenfassung:Hexamminechromium(III) hexamolybdocobaltate [Cr(NH 3 ) 6 ][CoMo 6 O 18 (OH) 6 ] · 5H 2 O was prepared and studied by mass spectrometry, IR spectroscopy, thermogravimetry, and powder X-ray diffraction. The crystals are monoclinic: a = 11.70 Å, b = 10.69 Å, c = 15.34 Å, β = 115.04°, V = 1905.11 Å 3 , ρ calcd . = 1.06 g/cm 3 , Z = 1.
ISSN:0036-0236
1531-8613
DOI:10.1134/S0036023613070176