Improvements in mechanical and thermo-mechanical properties of e-glass/epoxy composites using amino functionalized MWCNTs
The prime objective of this work is to optimize the mechanical and thermo-mechanical properties of e-glass/epoxy composites by utilizing amino-functionalized multi-walled carbon nanotubes (MWCNTs–NH2) through a combination of dispersion method. At first, 0.1–0.4wt.% of MWCNT–NH2 was integrated into...
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Veröffentlicht in: | Composite structures 2012-07, Vol.94 (8), p.2397-2406 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | The prime objective of this work is to optimize the mechanical and thermo-mechanical properties of e-glass/epoxy composites by utilizing amino-functionalized multi-walled carbon nanotubes (MWCNTs–NH2) through a combination of dispersion method. At first, 0.1–0.4wt.% of MWCNT–NH2 was integrated into SC-15 epoxy suspension using a combination of ultra-sonication and calendaring techniques. E-glass/epoxy nanocomposites were than fabricated at elevated temperature with the modified resin using hand layup and compression hot press. 3-Point flexural and dynamic mechanical analysis (DMA) results demonstrated a linearly increasing trend in properties from 0 to 0.3wt.% loading. Micrographs of MWCNTs incorporated epoxy and e-glass/epoxy samples revealed uniform dispersion of MWCNTs in epoxy, good interfacial adhesion between CNTs and polymer, and improved interfacial bonding between fiber/matrix at 0.3wt.% loading. An improved dispersion and hence an improved crosslink interaction between MWCNT–NH2 and epoxy lead to the stronger shift of the mechanical and thermo-mechanical properties of the composites. |
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ISSN: | 0263-8223 1879-1085 |
DOI: | 10.1016/j.compstruct.2012.03.014 |