Improvements in mechanical and thermo-mechanical properties of e-glass/epoxy composites using amino functionalized MWCNTs

The prime objective of this work is to optimize the mechanical and thermo-mechanical properties of e-glass/epoxy composites by utilizing amino-functionalized multi-walled carbon nanotubes (MWCNTs–NH2) through a combination of dispersion method. At first, 0.1–0.4wt.% of MWCNT–NH2 was integrated into...

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Veröffentlicht in:Composite structures 2012-07, Vol.94 (8), p.2397-2406
Hauptverfasser: Rahman, M.M., Zainuddin, S., Hosur, M.V., Malone, J.E., Salam, M.B.A., Kumar, Ashok, Jeelani, S.
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Sprache:eng
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Zusammenfassung:The prime objective of this work is to optimize the mechanical and thermo-mechanical properties of e-glass/epoxy composites by utilizing amino-functionalized multi-walled carbon nanotubes (MWCNTs–NH2) through a combination of dispersion method. At first, 0.1–0.4wt.% of MWCNT–NH2 was integrated into SC-15 epoxy suspension using a combination of ultra-sonication and calendaring techniques. E-glass/epoxy nanocomposites were than fabricated at elevated temperature with the modified resin using hand layup and compression hot press. 3-Point flexural and dynamic mechanical analysis (DMA) results demonstrated a linearly increasing trend in properties from 0 to 0.3wt.% loading. Micrographs of MWCNTs incorporated epoxy and e-glass/epoxy samples revealed uniform dispersion of MWCNTs in epoxy, good interfacial adhesion between CNTs and polymer, and improved interfacial bonding between fiber/matrix at 0.3wt.% loading. An improved dispersion and hence an improved crosslink interaction between MWCNT–NH2 and epoxy lead to the stronger shift of the mechanical and thermo-mechanical properties of the composites.
ISSN:0263-8223
1879-1085
DOI:10.1016/j.compstruct.2012.03.014