Flux growth and characterization of Sr sub(2)NiWO sub(6) single crystals
Single crystals of the double perovskite Sr sub(2)NiWO sub(6) were synthesized via SrCl sub(2) flux growth using high quality, phase-pure polycrystalline Sr sub(2)NiWO sub(6) as precursor material. This high quality precursor enabled us to grow large and phase pure crystals with sizes up to 1 mm x 1...
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Veröffentlicht in: | Journal of crystal growth 2015-07, Vol.421, p.39-44 |
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Hauptverfasser: | , , , , , , , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Single crystals of the double perovskite Sr sub(2)NiWO sub(6) were synthesized via SrCl sub(2) flux growth using high quality, phase-pure polycrystalline Sr sub(2)NiWO sub(6) as precursor material. This high quality precursor enabled us to grow large and phase pure crystals with sizes up to 1 mm x 1 mm in the basal plane and octahedral morphology. We measured the temperature dependence of the magnetization along the c-axis and along the ab plane. The analysis of the data allows a precise determination of the effective magnetic moment and the Curie-Weiss temperature. Sr sub(2)NiWO sub(6) orders antiferromagnetically at TN=54 K as revealed by magnetization and specific heat data. |
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ISSN: | 0022-0248 |
DOI: | 10.1016/j.jcrysgro.2015.04.004 |