An improved synthesis of [26-2H3]castasterone

Commercially available epicastasterone has been employed as a starting material for the preparation of [26‐2H3]castasterone. The chemical synthesis has been realized in 13 chemical steps and 4.6% total yield. The target compound is intended to be used as internal standard for the quantitative analys...

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Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 2015-11, Vol.58 (13-14), p.469-472
Hauptverfasser:	Zhabinskii, Vladimir N., Gulyakevich, Olga V., Kurman, Peter V., Shabunya, Polina S., Fatykhava, Svetlana A., Khripach, Vladimir A.
Format:	Artikel
Sprache:	eng
Schlagworte:	brassinosteroids castasterone Cholestanols - chemical synthesis Cholestanols - chemistry deuterium epicastasterone Radiopharmaceuticals - chemical synthesis Radiopharmaceuticals - chemistry synthesis Tritium - chemistry
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Beschreibung
Zusammenfassung:	Commercially available epicastasterone has been employed as a starting material for the preparation of [26‐2H3]castasterone. The chemical synthesis has been realized in 13 chemical steps and 4.6% total yield. The target compound is intended to be used as internal standard for the quantitative analysis of brassinosteroids. Commercially available epicastasterone has been employed as a starting material for the preparation of [26‐2H3]castasterone 1. The chemical synthesis has been realized in 13 chemical steps and 4.6% total yield. The target compound is intended to be used as internal standard for the quantitative analysis of brassinosteroids.
ISSN:	0362-4803 1099-1344
DOI:	10.1002/jlcr.3353