Synthesis of Pyrrolidinium Salts Using a Triazine-based Reagent under Mild Conditions

Synthesis of Pyrrolidinium Salts Using a Triazine-based Reagent under Mild Conditions

Various pyrrolidinium salts were synthesized from N,N-dialkyl-N′,N′-dimethylbutane-1,4-diamine using 2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT) under mild conditions. Cyclization reaction for the pyrrolidinium salts proceeded in high yields in polar solvents such as methanol and acetonitrile.

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Veröffentlicht in:Chemistry letters 2014, Vol.43 (10), p.1593-1595
Hauptverfasser: Kitamura, Masanori, Yamamura, Seina, Kobayashi, Hiroko, Yamamoto, Mariko, Tada, Kayo, Hioki, Kazuhito, Yamada, Kohei, Kunishima, Munetaka
Format: Artikel
Sprache:eng
Schlagworte:
Acetonitrile
Methyl alcohol
Solvents
Synthesis
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Zusammenfassung:Various pyrrolidinium salts were synthesized from N,N-dialkyl-N′,N′-dimethylbutane-1,4-diamine using 2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT) under mild conditions. Cyclization reaction for the pyrrolidinium salts proceeded in high yields in polar solvents such as methanol and acetonitrile.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.140503