Cyclodextrin Nitrate Ester/H sub(2)SO sub(4) as a Novel Nitrating System for Efficient Synthesis of Insensitive High Explosive 3-Nitro-1,2,4-triazol-5-one

Cyclodextrin Nitrate Ester/H sub(2)SO sub(4) as a Novel Nitrating System for Efficient Synthesis of Insensitive High Explosive 3-Nitro-1,2,4-triazol-5-one

A highly efficient and novel protocol for the synthesis of 3-nitro-1,2,4-triazol-5-one (NTO) using cyclodextrin nitrate ester (CDN) as a solid and safer catalyst is described.

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Industrial & engineering chemistry research 2014-12, Vol.53 (50), p.19375-19379
Hauptverfasser: Deshmukh, Mukesh B, Wagh, Nilesh D, Sikder, Arun K, Borse, Amulrao U, Dalal, Dipak S
Format: Artikel
Sprache:eng
Schlagworte:
Catalysts
Cyclodextrins
Explosions
Industrial engineering
Nitrate esters
Nitration
Synthesis
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:A highly efficient and novel protocol for the synthesis of 3-nitro-1,2,4-triazol-5-one (NTO) using cyclodextrin nitrate ester (CDN) as a solid and safer catalyst is described.
ISSN:0888-5885
1520-5045
DOI:10.1021/ie502555a