Investigation of flow parameters and efficiency of mixture separation on a structured packing

Results of experimental study of the effect of initial maldistribution of structured packing irrigation on efficiency of binary mixture separation are presented in this article. The studies were carried out in the experimental distillation column with the diameter of 0.9 m using the R114 and R21 freon mixture. Experiments were performed on the structured Mellapak 350.Y packing of stainless steel 316L, containing 19 layers with the total height of 4.016 m at the ratio of mole liquid and vapor flow rates L/V = 1 and 1.7, respectively, and the pressure in the upper part of the column ptop = 3 bars. Nonuniformity at the packing inlet was generated via the blocking of some holes in the liquid distributor. Here, we present some results on efficiency of mixture separation, pressure drop on the packing, distribution of local liquid flow rate under the packing over the cross‐section and on the column wall within the range of vapor loading factor (0.69