A New Quartz Crystal Microbalance Measuring Method with Expansive Frequency Range and Broadband Adaptive Response Capacity

In order to solve the problems of present quartz crystal microbalance (QCM) measuring instruments, such as high demand for crystal cutting technology and uncomprehensive measurements for crystal parameters, a modified quadrature demodulation-based method was proposed with broadband adaptive response...

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Veröffentlicht in:Fēnxī huàxué 2014-05, Vol.42 (5), p.773-778
Hauptverfasser: ZHOU, Jun-Peng, BAO, Yu, LIN, Qing, PANG, Ren-Shan, WANG, Lian-Ming, NIU, Li
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Sprache:eng
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Zusammenfassung:In order to solve the problems of present quartz crystal microbalance (QCM) measuring instruments, such as high demand for crystal cutting technology and uncomprehensive measurements for crystal parameters, a modified quadrature demodulation-based method was proposed with broadband adaptive response capacity and high frequency resolution. Moreover, it is also capable of measuring both resonant frequencies and dissipation factor D synchronously and continuously. Experimental results at room temperature indicated that the adaptive frequency range was 1-9 MHz while the frequency resolution was less than 1 Hz, measured resonance frequency shifts of crystals in the range scale linearly with the equal thickness increments of poly acrylic acid (PAA) membrane on the working electrode, and with the volatilization of different solvent factor D is measured continuously and effectively along the time axis. To sum up, compared with traditional ones, this new method has lower material cost and more obtained parameters.
ISSN:0253-3820
DOI:10.3724/SP.J.1096.2014.40061