Facile synthesis of pure 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxy bisanhydride and bisimide

Facile synthesis of pure 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxy bisanhydride and bisimide

A robust and scalable procedure to obtain pure 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxy bisanhydride, a highly valuable synthon, has been developed via synthesis of a novel intermediate compound 1,6,7,12-perylene-3,4,9,10-tetracarboxy tetrabutylester.

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Veröffentlicht in:Organic letters 2015-04, Vol.17 (8), p.1882-1885
Hauptverfasser: Dubey, Rajeev K, Westerveld, Nick, Grozema, Ferdinand C, Sudhölter, Ernst J R, Jager, Wolter F
Format: Artikel
Sprache:eng
Schlagworte:
Imides - chemical synthesis
Imides - chemistry
Molecular Structure
Perylene - analogs & derivatives
Perylene - chemical synthesis
Perylene - chemistry
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Zusammenfassung:A robust and scalable procedure to obtain pure 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxy bisanhydride, a highly valuable synthon, has been developed via synthesis of a novel intermediate compound 1,6,7,12-perylene-3,4,9,10-tetracarboxy tetrabutylester.
ISSN:1523-7060
1523-7052
DOI:10.1021/acs.orglett.5b00562