Dry-gel conversion synthesis of Cr-MIL-101 aided by grinding: high surface area and high yield synthesis with minimum purification

Dry-gel conversion synthesis of Cr-MIL-101 aided by grinding: high surface area and high yield synthesis with minimum purification

A dry gel conversion synthesis aided by fine-grinding of the synthesis precursors produces a MIL-101 product with a high surface area greater than 4100 m(2) g(-1) and a product yield approaching 90% in a very reproducible manner after only simple water washing.

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Bibliographische Detailangaben
Veröffentlicht in:Chemical communications (Cambridge, England) England), 2013-09, Vol.49 (69), p.7647-7649
Hauptverfasser: Kim, Jun, Lee, Yu-Ri, Ahn, Wha-Seung
Format: Artikel
Sprache:eng
Schlagworte:
Chromium
Conversion
Drying
Precursors
Purification
Surface area
Synthesis
Washing
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Beschreibung
Zusammenfassung:A dry gel conversion synthesis aided by fine-grinding of the synthesis precursors produces a MIL-101 product with a high surface area greater than 4100 m(2) g(-1) and a product yield approaching 90% in a very reproducible manner after only simple water washing.
ISSN:1359-7345
1364-548X
DOI:10.1039/c3cc44559c