Thermal decomposition of tetraethyl ammonium tetrafluoroborate

Thermal decomposition of tetraethyl ammonium tetrafluoroborate

Thermal decomposition of tetraethyl ammonium tetrafluoroborate has been studied employing simultaneous techniques of TG-DTG-DSC-quadrupole mass spectrometric techniques in an inert atmosphere of pure Helium gas at a sample heating rate of 5 K min-1 employing a platinum crucible. The observed decompo...

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Veröffentlicht in:Journal of thermal analysis and calorimetry 2014-02, Vol.115 (2), p.1901-1905
Hauptverfasser: Prasad, M, Sudhakarbabu, K
Format: Artikel
Sprache:eng
Schlagworte:
Calorimetry
Crucibles
Heating rate
Helium
Inert atmospheres
Platinum
Spectroscopy
Thermal decomposition
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Zusammenfassung:Thermal decomposition of tetraethyl ammonium tetrafluoroborate has been studied employing simultaneous techniques of TG-DTG-DSC-quadrupole mass spectrometric techniques in an inert atmosphere of pure Helium gas at a sample heating rate of 5 K min-1 employing a platinum crucible. The observed decomposition paths are the most commonly expected Hofmann elimination and substitution reactions paths.
ISSN:1388-6150
1572-8943
DOI:10.1007/s10973-013-3378-7