Formation of ZnO within flexible polymer fibers
In the process of fiber production from Zinc acetate and Polyvinylpyrrolidone using the electrospinning method, ZnO forms at temperature as low as 120 °C. The fibers were characterized using scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and ultraviolet–vis...
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Veröffentlicht in: | Journal of sol-gel science and technology 2013-02, Vol.65 (2), p.283-286 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | In the process of fiber production from Zinc acetate and Polyvinylpyrrolidone using the electrospinning method, ZnO forms at temperature as low as 120 °C. The fibers were characterized using scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and ultraviolet–visible (UV–Vis) spectroscopy. Upon heating at 120 °C for 12 h some fibers shrink in diameter down to about 100 nm while others remain in the 400–900 nm range. Within the hybrid fibers, ZnO crystallizes in the wurtzite structure with a bang gap of 3.3 eV. The hybrid fibers exhibit the flexibility of polymer component and optical properties of ZnO phase, and promise to be very useful in various applications. |
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ISSN: | 0928-0707 1573-4846 |
DOI: | 10.1007/s10971-012-2928-y |