Formation of ZnO within flexible polymer fibers

In the process of fiber production from Zinc acetate and Polyvinylpyrrolidone using the electrospinning method, ZnO forms at temperature as low as 120 °C. The fibers were characterized using scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and ultraviolet–vis...

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Veröffentlicht in:Journal of sol-gel science and technology 2013-02, Vol.65 (2), p.283-286
Hauptverfasser: Turinske, Alexander J., Nelson, Scott A., Stojilovic, Nenad, Ali, Sulaiman B., Dordevic, Sasa V., Evans, Edward A.
Format: Artikel
Sprache:eng
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Zusammenfassung:In the process of fiber production from Zinc acetate and Polyvinylpyrrolidone using the electrospinning method, ZnO forms at temperature as low as 120 °C. The fibers were characterized using scanning electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and ultraviolet–visible (UV–Vis) spectroscopy. Upon heating at 120 °C for 12 h some fibers shrink in diameter down to about 100 nm while others remain in the 400–900 nm range. Within the hybrid fibers, ZnO crystallizes in the wurtzite structure with a bang gap of 3.3 eV. The hybrid fibers exhibit the flexibility of polymer component and optical properties of ZnO phase, and promise to be very useful in various applications.
ISSN:0928-0707
1573-4846
DOI:10.1007/s10971-012-2928-y