Obtainment of the Fe0.70−xCrxAl0.3/Al2O3 nanocomposite by the method of SHS of mechanoactivated Cr2O3 + Fe + Al mixtures
Applying Mössbauer spectroscopy methods, we have studied the structure of nanocomposites obtained by a technique combining the preliminary mechanical activation of an 8.1 wt % Cr 2 O 3 + 65.9 wt % Fe + 25 wt % Al mixture and self-propagating high-temperature synthesis (SHS). It has been found that,...
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Veröffentlicht in: | Inorganic materials 2009-07, Vol.45 (7), p.827-831 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | Applying Mössbauer spectroscopy methods, we have studied the structure of nanocomposites obtained by a technique combining the preliminary mechanical activation of an 8.1 wt % Cr
2
O
3
+ 65.9 wt % Fe + 25 wt % Al mixture and self-propagating high-temperature synthesis (SHS). It has been found that, at the stage of mechanical activation, an Fe/Al/Cr
2
O
3
composite with a low impurity of the Fe
2
Al
5
intermetallide is formed. At the stage of SHS, the interaction between activated components of the mixture leads to the formation of the Fe
0.7 −
x
Cr
x
Al
0.3
(
x
= 0 − 0.2)/Al
2
O
3
composite. |
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ISSN: | 0020-1685 1608-3172 |
DOI: | 10.1134/S002016850907022X |