Direct synthesis of nano-sized glass powders with spherical shape by RF (radio frequency) thermal plasma
A new route for obtaining very small, spheroid glass powders is demonstrated using an RF (radio frequency) thermal plasma system. During the process, four kinds of chemicals, here SiO 2, B 2O 3, BaCO 3, and K 2CO 3, were mixed at pre-set weight ratios, spray-dried, calcined at 250 °C for 3 h, and cr...
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Veröffentlicht in: | Thin solid films 2011-08, Vol.519 (20), p.7111-7115 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | A new route for obtaining very small, spheroid glass powders is demonstrated using an RF (radio frequency) thermal plasma system. During the process, four kinds of chemicals, here SiO
2, B
2O
3, BaCO
3, and K
2CO
3, were mixed at pre-set weight ratios, spray-dried, calcined at 250
°C for 3
h, and crushed into fragments. Then, they were successfully reformed into nano-sized amorphous powders (<
200
nm) with spherical shape by injecting them along the centerline of an RF thermal plasma reactor at ~
24
kW. The as-synthesized powders show negligible (<
1%) composition changes when compared with the injected precursors of raw material compounds. |
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ISSN: | 0040-6090 1879-2731 |
DOI: | 10.1016/j.tsf.2011.01.215 |