Validation of a high performance liquid chromatographic method for alpha amanitin determination in urine

The objective of the present study was to develop and validate a liquid chromatographic method with electrochemical detection to measure alpha amanitin concentrations in urine after sample pretreatment with double mechanism (reversed phase/cation exchange) solid-phase extraction cartridges. The urin...

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Veröffentlicht in:	Forensic science international 1998-03, Vol.92 (1), p.59-68
Hauptverfasser:	Defendenti, C, Bonacina, E, Mauroni, M, Gelosa, L
Format:	Artikel
Sprache:	eng
Schlagworte:	Accuracy Acetonitrile Alpha amanitin Amanitin Amanitins - chemistry Amanitins - urine Biological and medical sciences Cation exchange Cation exchanging Chromatography Chromatography, High Pressure Liquid - methods Chromatography, High Pressure Liquid - standards Coefficient of variation Column chromatography Column liquid chromatography Contaminants Electrochemical analysis Electrochemical detection Electrochemistry Electrodes Forensic Medicine Humans Intoxication Mathematical analysis Medical sciences Mushroom Poisoning - urine Mushrooms Oxidation Plant poisons toxicology Poisoning Reproducibility of Results RNA polymerase Signal to noise ratio Solid phases Toxicology Urination Urine
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