Processing of Lovage into High-Value Components Using Supercritical CO sub(2) and Pressurized Liquid Extraction
Lovage roots, leaves, and stems were extracted by supercritical carbon dioxide (SFE-CO sub(2)), while the residues of SFE-CO sub(2) were further extracted by pressurized liquid extraction with acetone and methanol. Optimization of SFE-CO sub(2) parameters resulted in enhanced extract yields from all...
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Veröffentlicht in: | Chemical engineering & technology 2014-11, Vol.37 (11), p.1854-1860 |
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creator | Kemzurait, Aurelija Venskutonis, Petras R Navikien, Diana |
description | Lovage roots, leaves, and stems were extracted by supercritical carbon dioxide (SFE-CO sub(2)), while the residues of SFE-CO sub(2) were further extracted by pressurized liquid extraction with acetone and methanol. Optimization of SFE-CO sub(2) parameters resulted in enhanced extract yields from all lovage parts. The antioxidant potential of solid material and extracts was assessed by Trolox-equivalent antioxidant capacity (TEAC) in two different assays and by the total phenolic content (TPC). TEAC and TPC values of SFE-CO sub(2) residues were distinctly lower than those of the initial lovage material which indicates that lovage antioxidants are distributed both in lipophilic and fat-insoluble fractions. High-pressure techniques, namely supercritical CO sub(2) and pressurized liquid extraction, demonstrate the potential to significantly increase the efficiency of processing of different anatomical parts of lovage into high-value fractions based on their solubility in nonpolar (CO sub(2)) and protonic (methanol/water) solvents under supercritical and subcritical conditions. |
doi_str_mv | 10.1002/ceat.201300735 |
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Optimization of SFE-CO sub(2) parameters resulted in enhanced extract yields from all lovage parts. The antioxidant potential of solid material and extracts was assessed by Trolox-equivalent antioxidant capacity (TEAC) in two different assays and by the total phenolic content (TPC). TEAC and TPC values of SFE-CO sub(2) residues were distinctly lower than those of the initial lovage material which indicates that lovage antioxidants are distributed both in lipophilic and fat-insoluble fractions. High-pressure techniques, namely supercritical CO sub(2) and pressurized liquid extraction, demonstrate the potential to significantly increase the efficiency of processing of different anatomical parts of lovage into high-value fractions based on their solubility in nonpolar (CO sub(2)) and protonic (methanol/water) solvents under supercritical and subcritical conditions.</description><identifier>ISSN: 0930-7516</identifier><identifier>EISSN: 1521-4125</identifier><identifier>DOI: 10.1002/ceat.201300735</identifier><language>eng</language><subject>Acetone ; Antioxidants ; Carbon dioxide ; Chemical engineering ; Extraction ; Liquids ; Methyl alcohol ; Residues</subject><ispartof>Chemical engineering & technology, 2014-11, Vol.37 (11), p.1854-1860</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Kemzurait, Aurelija</creatorcontrib><creatorcontrib>Venskutonis, Petras R</creatorcontrib><creatorcontrib>Navikien, Diana</creatorcontrib><title>Processing of Lovage into High-Value Components Using Supercritical CO sub(2) and Pressurized Liquid Extraction</title><title>Chemical engineering & technology</title><description>Lovage roots, leaves, and stems were extracted by supercritical carbon dioxide (SFE-CO sub(2)), while the residues of SFE-CO sub(2) were further extracted by pressurized liquid extraction with acetone and methanol. Optimization of SFE-CO sub(2) parameters resulted in enhanced extract yields from all lovage parts. The antioxidant potential of solid material and extracts was assessed by Trolox-equivalent antioxidant capacity (TEAC) in two different assays and by the total phenolic content (TPC). TEAC and TPC values of SFE-CO sub(2) residues were distinctly lower than those of the initial lovage material which indicates that lovage antioxidants are distributed both in lipophilic and fat-insoluble fractions. High-pressure techniques, namely supercritical CO sub(2) and pressurized liquid extraction, demonstrate the potential to significantly increase the efficiency of processing of different anatomical parts of lovage into high-value fractions based on their solubility in nonpolar (CO sub(2)) and protonic (methanol/water) solvents under supercritical and subcritical conditions.</description><subject>Acetone</subject><subject>Antioxidants</subject><subject>Carbon dioxide</subject><subject>Chemical engineering</subject><subject>Extraction</subject><subject>Liquids</subject><subject>Methyl alcohol</subject><subject>Residues</subject><issn>0930-7516</issn><issn>1521-4125</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqVjMtKAzEUQIMoOD62ru-yLqbem5g-1kOli4IFW7clZm7HyDSZ5iHi11vEH3B1OHA4QtwRjglRPlg2eSyRFOJU6TNRkZZUP5LU56LCucJ6qmlyKa5S-kBEOkklwjoGyyk530HYwyp8mo7B-Rxg6br3-tX0haEJhyF49jnB9jd9KQNHG1121vTQPEMqbyN5D8a3sI6nX4num1tYuWNxLSy-cjQ2u-BvxMXe9Ilv_3gtRk-LTbOshxiOhVPeHVyy3PfGcyhpRxM5V3pGM1L_SH8AzbZUTw</recordid><startdate>20141101</startdate><enddate>20141101</enddate><creator>Kemzurait, Aurelija</creator><creator>Venskutonis, Petras R</creator><creator>Navikien, Diana</creator><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20141101</creationdate><title>Processing of Lovage into High-Value Components Using Supercritical CO sub(2) and Pressurized Liquid Extraction</title><author>Kemzurait, Aurelija ; Venskutonis, Petras R ; Navikien, Diana</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_miscellaneous_16293581813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Acetone</topic><topic>Antioxidants</topic><topic>Carbon dioxide</topic><topic>Chemical engineering</topic><topic>Extraction</topic><topic>Liquids</topic><topic>Methyl alcohol</topic><topic>Residues</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kemzurait, Aurelija</creatorcontrib><creatorcontrib>Venskutonis, Petras R</creatorcontrib><creatorcontrib>Navikien, Diana</creatorcontrib><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Chemical engineering & technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kemzurait, Aurelija</au><au>Venskutonis, Petras R</au><au>Navikien, Diana</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Processing of Lovage into High-Value Components Using Supercritical CO sub(2) and Pressurized Liquid Extraction</atitle><jtitle>Chemical engineering & technology</jtitle><date>2014-11-01</date><risdate>2014</risdate><volume>37</volume><issue>11</issue><spage>1854</spage><epage>1860</epage><pages>1854-1860</pages><issn>0930-7516</issn><eissn>1521-4125</eissn><abstract>Lovage roots, leaves, and stems were extracted by supercritical carbon dioxide (SFE-CO sub(2)), while the residues of SFE-CO sub(2) were further extracted by pressurized liquid extraction with acetone and methanol. Optimization of SFE-CO sub(2) parameters resulted in enhanced extract yields from all lovage parts. The antioxidant potential of solid material and extracts was assessed by Trolox-equivalent antioxidant capacity (TEAC) in two different assays and by the total phenolic content (TPC). TEAC and TPC values of SFE-CO sub(2) residues were distinctly lower than those of the initial lovage material which indicates that lovage antioxidants are distributed both in lipophilic and fat-insoluble fractions. High-pressure techniques, namely supercritical CO sub(2) and pressurized liquid extraction, demonstrate the potential to significantly increase the efficiency of processing of different anatomical parts of lovage into high-value fractions based on their solubility in nonpolar (CO sub(2)) and protonic (methanol/water) solvents under supercritical and subcritical conditions.</abstract><doi>10.1002/ceat.201300735</doi></addata></record> |
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subjects | Acetone Antioxidants Carbon dioxide Chemical engineering Extraction Liquids Methyl alcohol Residues |
title | Processing of Lovage into High-Value Components Using Supercritical CO sub(2) and Pressurized Liquid Extraction |
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