A simple method for synthesis and isolation of single PCB congeners shown by the example of PCB 132, a possible interference of PCB 153 and PCB 105

A simple method for synthesis and isolation of single PCB congeners shown by the example of PCB 132, a possible interference of PCB 153 and PCB 105

PCB 132 was prepared by Cadogan coupling [1] and isolated by semi-preparative RP-HPLC in purity larger than 98%. The GC separation of the PCB 153, 132, and 105 on different silica fused columns (Ultra-2, HP-5, OV-1701, OV-210, OV-225) was discussed.

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Veröffentlicht in:Chemosphere (Oxford) 1991, Vol.23 (2), p.193-198
Hauptverfasser: Vetter, Walter, Luckas, Bernd, Haubold, Wolfgang
Format: Artikel
Sprache:eng
Schlagworte:
Analytical chemistry
Chemistry
Exact sciences and technology
Miscellaneous
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Zusammenfassung:PCB 132 was prepared by Cadogan coupling [1] and isolated by semi-preparative RP-HPLC in purity larger than 98%. The GC separation of the PCB 153, 132, and 105 on different silica fused columns (Ultra-2, HP-5, OV-1701, OV-210, OV-225) was discussed.
ISSN:0045-6535
1879-1298
DOI:10.1016/0045-6535(91)90106-N