Optimization of ultrasound-assisted extraction of polyphenols from spruce wood bark
•Spruce bark (picea abies) is a rich source of phenolic compounds with antioxidant activity.•Non-toxic solvent was used (ethanol and water).•Effects of ultrasound-assisted extraction as influenced by time, temperature and ethanol concentration were evaluated.•Polyphenols extraction is improved by ul...
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Veröffentlicht in: | Ultrasonics sonochemistry 2015-01, Vol.22, p.535-541 |
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Sprache: | eng |
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Zusammenfassung: | •Spruce bark (picea abies) is a rich source of phenolic compounds with antioxidant activity.•Non-toxic solvent was used (ethanol and water).•Effects of ultrasound-assisted extraction as influenced by time, temperature and ethanol concentration were evaluated.•Polyphenols extraction is improved by ultrasound assisted extraction with 70% ethanol.•The highest yield of total polyphenols obtained by ANOVA factorial was 13.232mgGAE/g spruce wood bark.
Here we describe the ultrasound-assisted extraction of the phenolic compounds from spruce wood bark and present a straight-forward experimental planning method, allowing the optimisation of the process. The effect of ethanol concentration, temperature and extraction time were evaluated through a 32·2 experimental planning. The efficiency of the extraction process was appreciated based on factorial ANOVA results. The maximum extraction yield of total polyphenols (13.232mg gallic acid equivalents (GAE)/g of spruce bark tested) was obtained using a process time of 60min, an extraction temperature of 54°C and a concentration of ethanol of 70% respectively. These results indicate that an important quantity of bioactive compounds can be extracted from spruce wood bark by ultrasound assisted extraction technology. |
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ISSN: | 1350-4177 1873-2828 |
DOI: | 10.1016/j.ultsonch.2014.07.013 |