Functionalization and dispersion of multiwalled carbon nanotubes modified with poly- l -lysine

Poly-l-lysine (PLL) was synthesized using lysine as raw material by N-carboxyanhydride polymerization and characterized by Fourier transform infrared spectroscopy and 1H NMR. Multiwalled carbon nanotubes (MWCNTs) were non-covalently functionalized using PLL in order to prepare MWCNTs-PLL composite....

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Colloids and surfaces. A, Physicochemical and engineering aspects Physicochemical and engineering aspects, 2014-02, Vol.443, p.19-26
Hauptverfasser: Ling, Xinlong, Wei, Yizhe, Zou, Liming, Xu, Su
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:Poly-l-lysine (PLL) was synthesized using lysine as raw material by N-carboxyanhydride polymerization and characterized by Fourier transform infrared spectroscopy and 1H NMR. Multiwalled carbon nanotubes (MWCNTs) were non-covalently functionalized using PLL in order to prepare MWCNTs-PLL composite. MWCNTs-PLL was characterized using Fourier transform infrared spectroscopy, thermogravimetric analysis and UV-Vis absorption spectroscopy. The dispersion of MWCNTs-PLL composite was investigated by UV-Vis absorption spectroscopy, dynamic light scattering analysis and digital photograph. The results showed that the dispersion of MWCNTs-PLL composite was obviously better than that of MWCNTs-SDS composite in water while it was also approximate with that of MWCNTs-SDBS. In addition, MWCNTs-PLL was pH-responsive in water so that it could be used as bio-nanomaterial in future.
ISSN:0927-7757
DOI:10.1016/j.colsurfa.2013.10.053