A simple and economic method for accurate determination of the energy peak efficiency of 208 keV γ-ray of 237U based on 241Pu/237U secular equilibrium
A new method is developed for the determination of energy peak efficiency of 208 keV γ-ray of 237 U based on 241 Pu/ 237 U secular equilibrium. Plutonium solution was purified to remove Am with Dowex 1 × 2 anion exchange chromatography and the concentration of 241 Pu in the purified solution was det...
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Veröffentlicht in: | Journal of radioanalytical and nuclear chemistry 2014-03, Vol.299 (3), p.1987-1991 |
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Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | A new method is developed for the determination of energy peak efficiency of 208 keV γ-ray of
237
U based on
241
Pu/
237
U secular equilibrium. Plutonium solution was purified to remove Am with Dowex 1 × 2 anion exchange chromatography and the concentration of
241
Pu in the purified solution was determined using
242
Pu isotope-dilution mass spectrometry on an inductively-coupled plasma mass spectrometry. The solution can be used as calibration source for the determination of energy peak efficiency of 208 keV γ-ray of
237
U after 48 days. The method was validated for a planar HPGe detector at the 12 mm above the detector surface. The results showed that this is a simple and economic method for determining the energy peak efficiency of gamma detectors for 208 keV γ-ray of
237
U. |
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ISSN: | 0236-5731 1588-2780 |
DOI: | 10.1007/s10967-014-2937-0 |