Investigation of dislocation structures in ribbon- and ingot-grown multicrystalline silicon

In this paper, an experimental study of dislocation structures in multicrystalline silicon is presented. The alignment of dislocations in samples from both edge-defined film-fed growth and ingot crystallization by vertical Bridgman growth is investigated. Crystallographic orientations of single grai...

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Veröffentlicht in:Journal of crystal growth 2013-11, Vol.382, p.41-46
Hauptverfasser: Schmid, E., Funke, C., Behm, T., Pätzold, O., Berek, H., Stelter, M.
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Sprache:eng
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Zusammenfassung:In this paper, an experimental study of dislocation structures in multicrystalline silicon is presented. The alignment of dislocations in samples from both edge-defined film-fed growth and ingot crystallization by vertical Bridgman growth is investigated. Crystallographic orientations of single grains and dislocation structures are analyzed by electron backscatter diffraction and infrared microscopy. {111} and {211} planes are identified to be the typical crystallographic planes, where dislocations are arranged. It is concluded that {111} and {211} planes are involved in plastic deformation and recovery processes during growth, respectively. In ribbon-grown samples, the dislocations are mainly arranged on {111} slip planes, whereas an arrangement on {211} planes prevails in ingot-grown samples. The influence of the growth and cooling conditions on the final alignment of dislocations in mc-Si is discussed and a possible explanation for a different annealing behaviour of ribbon- and ingot-grown crystals is given. •Dislocation structures in ribbon- and ingot-grown mc-Si are studied systematically.•{111} and {211} planes are identified to be the characteristic crystallographic planes, where dislocations are arranged.•A dislocation arrangement in {111} planes results from plastic deformation, while an arrangement in {211} planes can be attributed to recovery processes.•Growth and cooling conditions play a major role for the alignment and annealing behaviour of dislocations in mc-Si crystals.
ISSN:0022-0248
1873-5002
DOI:10.1016/j.jcrysgro.2013.07.036