Towards scalable production of polyamide 12/halloysite nanocomposites via water-assisted extrusion: mechanical modeling, thermal and fire properties

In this study, polyamide 12 (PA12)/untreated halloysite nanotubes (HNTs) nanocomposites are prepared in a semi‐industrial scale extruder using a non‐traditional “one step” water‐assisted extrusion process. A morphological study is carried out using a combination of scanning electron microscopy and t...

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Veröffentlicht in:Polymers for advanced technologies 2014-02, Vol.25 (2), p.137-151
Hauptverfasser: Lecouvet, B., Sclavons, M., Bourbigot, S., Bailly, C.
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Sprache:eng
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Zusammenfassung:In this study, polyamide 12 (PA12)/untreated halloysite nanotubes (HNTs) nanocomposites are prepared in a semi‐industrial scale extruder using a non‐traditional “one step” water‐assisted extrusion process. A morphological study is carried out using a combination of scanning electron microscopy and transmission electron microscopy analyses to evaluate the influence of water injection and filler content on the quality of clay dispersion. The use of water injection slightly improves the nanoscale dispersion at low HNTs content (
ISSN:1042-7147
1099-1581
DOI:10.1002/pat.3215