Thermal behavior of BST//PVDF ceramicapolymer composites
In this paper, we report the results of a study of microstructure and thermal behavior of ceramicapolymer composites composed of barium strontium titanate Ba0.6Sr0.4TiO3 (BST60/40) and polyvinylidene fluoride (PVDF). The Ba0.6Sr0.4TiO3 ceramic powder was prepared by the sol-gel method. Thermal evolu...
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Veröffentlicht in: | Journal of thermal analysis and calorimetry 2013-07, Vol.113 (1), p.69-76 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | In this paper, we report the results of a study of microstructure and thermal behavior of ceramicapolymer composites composed of barium strontium titanate Ba0.6Sr0.4TiO3 (BST60/40) and polyvinylidene fluoride (PVDF). The Ba0.6Sr0.4TiO3 ceramic powder was prepared by the sol-gel method. Thermal evolution of the dried gel as well as ceramic powder was studied by simultaneous thermal analysis. The composite BST60/40//PVDF was obtained by hot pressing method for volume fraction of BST60/40 ceramic powder c v = 50 %. The morphology of BST60/40//PVDF composite powder was observed by transmission electron microscopy and the morphology of BST60/40//PVDF composite sample was observed by scanning electron microscopy. Temperature dependence of dielectric constant and dielectric loss factor of BST60/40//PVDF composites was measured in the frequency range of f = (10 A 103a1 A 106) Hz. Dynamic mechanical properties of BST60/40//PVDF composites were measured by dynamic mechanical thermal analysis DMTA. |
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ISSN: | 1388-6150 1572-8943 |
DOI: | 10.1007/s10973-013-3026-2 |