A benign synthesis of 2-amino-4H-chromene in aqueous medium using hydrotalcite (HT) as a heterogeneous base catalyst
A simple and environmentally benign synthesis of 2-amino-4H-chromene is described using hydrotalcite as a solid base catalyst in aqueous medium. The catalysts were prepared by a co-precipitation method and well characterized by various techniques such as XRD, FT-IR, SEM and the basicity was found us...
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Veröffentlicht in: | Catalysis science & technology 2013-01, Vol.3 (8), p.2050-2056 |
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Hauptverfasser: | , , , , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | A simple and environmentally benign synthesis of 2-amino-4H-chromene is described using hydrotalcite as a solid base catalyst in aqueous medium. The catalysts were prepared by a co-precipitation method and well characterized by various techniques such as XRD, FT-IR, SEM and the basicity was found using the phenol adsorption method. The reusability of the catalyst, use of water as a green solvent and easy isolation of the product along with good yields make the present protocol sustainable and advantageous compared to conventional methods. |
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ISSN: | 2044-4753 2044-4761 |
DOI: | 10.1039/c3cy20856g |