A 30 nm-resolution hard X-ray microscope with X-ray fluorescence mapping capability at BSRF

A full‐field transmission X‐ray microscope (TXM) operating continuously from 5 keV to 12 keV with fluorescence mapping capability has been designed and constructed at the Beijing Synchrotron Radiation Facility, a first‐generation synchrotron radiation facility operating at 2.5 GeV. Spatial resolutio...

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Veröffentlicht in:Journal of synchrotron radiation 2012-11, Vol.19 (6), p.1021-1028
Hauptverfasser: Yuan, Qingxi, Zhang, Kai, Hong, Youli, Huang, Wanxia, Gao, Kun, Wang, Zhili, Zhu, Peiping, Gelb, Jeff, Tkachuk, Andrei, Hornberger, Benjamin, Feser, Michael, Yun, Wenbing, Wu, Ziyu
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Sprache:eng
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Zusammenfassung:A full‐field transmission X‐ray microscope (TXM) operating continuously from 5 keV to 12 keV with fluorescence mapping capability has been designed and constructed at the Beijing Synchrotron Radiation Facility, a first‐generation synchrotron radiation facility operating at 2.5 GeV. Spatial resolution better than 30 nm has been demonstrated using a Siemens star pattern in both absorption mode and Zernike phase‐contrast mode. A scanning‐probe mode fluorescence mapping capability integrated with the TXM has been shown to provide 50 p.p.m. sensitivity for trace elements with a spatial resolution (limited by probing beam spot size) of 20 µm. The optics design, testing of spatial resolution and fluorescence sensitivity are presented here, including performance measurement results.
ISSN:1600-5775
0909-0495
1600-5775
DOI:10.1107/S0909049512032852