A 30 nm-resolution hard X-ray microscope with X-ray fluorescence mapping capability at BSRF
A full‐field transmission X‐ray microscope (TXM) operating continuously from 5 keV to 12 keV with fluorescence mapping capability has been designed and constructed at the Beijing Synchrotron Radiation Facility, a first‐generation synchrotron radiation facility operating at 2.5 GeV. Spatial resolutio...
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Veröffentlicht in: | Journal of synchrotron radiation 2012-11, Vol.19 (6), p.1021-1028 |
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Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | A full‐field transmission X‐ray microscope (TXM) operating continuously from 5 keV to 12 keV with fluorescence mapping capability has been designed and constructed at the Beijing Synchrotron Radiation Facility, a first‐generation synchrotron radiation facility operating at 2.5 GeV. Spatial resolution better than 30 nm has been demonstrated using a Siemens star pattern in both absorption mode and Zernike phase‐contrast mode. A scanning‐probe mode fluorescence mapping capability integrated with the TXM has been shown to provide 50 p.p.m. sensitivity for trace elements with a spatial resolution (limited by probing beam spot size) of 20 µm. The optics design, testing of spatial resolution and fluorescence sensitivity are presented here, including performance measurement results. |
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ISSN: | 1600-5775 0909-0495 1600-5775 |
DOI: | 10.1107/S0909049512032852 |