Influence of microwave technology on cocarboxylase hydrochloride particle diversity and drying efficiency
Two possible ways of crystallite downsizing of cocarboxylase hydrochloride namely mechanical milling and precipitation under high supersaturation conditions were studied as well as their influence on the drying parameters of the produced powders. It was found that both methods allowed shortening dry...
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| Veröffentlicht in: | Powder technology 2011-02, Vol.207 (1-3), p.134-139 |
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| container_title | Powder technology |
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| creator | Pinchukova, Natalia A. Chebanov, Valentin A. Danilina, Viktoria V. Desenko, Sergey M. Seminozhenko, Volodymyr P. Shishkin, Oleg V. Voloshko, Alexander Yu |
| description | Two possible ways of crystallite downsizing of cocarboxylase hydrochloride namely mechanical milling and precipitation under high supersaturation conditions were studied as well as their influence on the drying parameters of the produced powders. It was found that both methods allowed shortening drying times of powders. However, precipitation from highly supersaturated solutions was found to have a more significant effect on cocarboxylase hydrochloride drying in comparison with the milling as the crystallites produced by the former method have smaller sizes ( |
| doi_str_mv | 10.1016/j.powtec.2010.10.018 |
| format | Article |
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Drying times of cocarboxylase hydrochloride powders have been shown to be strongly dependant on particle diversity. Both mechanical milling of the powders obtained via uncontrollable crystallization and precipitation from highly supersaturated aqueous solutions have resulted in fine powders and considerable drying time shortening, the latter technique, however, demonstrated much more striking effect. [Display omitted]
► Microwave-assisted evaporation resulted in highly supersaturated solutions. ► Precipitation from highly supersaturated solutions resulted in very fine powders. ► Obtaining very fine powders allowed drying acceleration by the factor of 7. ► Application of microwave technologies will increase processes efficiency.</description><identifier>ISSN: 0032-5910</identifier><identifier>EISSN: 1873-328X</identifier><identifier>DOI: 10.1016/j.powtec.2010.10.018</identifier><identifier>CODEN: POTEBX</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Applied sciences ; Chemical engineering ; Crystallites ; Drying ; Evaporation ; Exact sciences and technology ; Hydrochlorides ; Inclusion ; Mechanical milling ; Microwave irradiation ; Microwaves ; Milling ; Miscellaneous ; Precipitation ; Solid-solid systems ; Supersaturation</subject><ispartof>Powder technology, 2011-02, Vol.207 (1-3), p.134-139</ispartof><rights>2010 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c369t-2e6e2df8632354a91a38fda5c25a623200e00528dd426b8e59138c3d4c047d8c3</citedby><cites>FETCH-LOGICAL-c369t-2e6e2df8632354a91a38fda5c25a623200e00528dd426b8e59138c3d4c047d8c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.powtec.2010.10.018$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23840052$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Pinchukova, Natalia A.</creatorcontrib><creatorcontrib>Chebanov, Valentin A.</creatorcontrib><creatorcontrib>Danilina, Viktoria V.</creatorcontrib><creatorcontrib>Desenko, Sergey M.</creatorcontrib><creatorcontrib>Seminozhenko, Volodymyr P.</creatorcontrib><creatorcontrib>Shishkin, Oleg V.</creatorcontrib><creatorcontrib>Voloshko, Alexander Yu</creatorcontrib><title>Influence of microwave technology on cocarboxylase hydrochloride particle diversity and drying efficiency</title><title>Powder technology</title><description>Two possible ways of crystallite downsizing of cocarboxylase hydrochloride namely mechanical milling and precipitation under high supersaturation conditions were studied as well as their influence on the drying parameters of the produced powders. It was found that both methods allowed shortening drying times of powders. However, precipitation from highly supersaturated solutions was found to have a more significant effect on cocarboxylase hydrochloride drying in comparison with the milling as the crystallites produced by the former method have smaller sizes (<10μm) without additional disintegration and contain much less inclusions of mother liquor. Obtaining solutions with high supersaturation degrees was achieved due to application of microwave irradiation at the evaporation stage that provided uniform gradientless heating of cocarboxylase aqueous solutions. The results of this work can be applied for producing other fine-crystalline substances and materials when particle sizes play a key role in the manufacture of products with the desired qualitative characteristics.
Drying times of cocarboxylase hydrochloride powders have been shown to be strongly dependant on particle diversity. Both mechanical milling of the powders obtained via uncontrollable crystallization and precipitation from highly supersaturated aqueous solutions have resulted in fine powders and considerable drying time shortening, the latter technique, however, demonstrated much more striking effect. [Display omitted]
► Microwave-assisted evaporation resulted in highly supersaturated solutions. ► Precipitation from highly supersaturated solutions resulted in very fine powders. ► Obtaining very fine powders allowed drying acceleration by the factor of 7. ► Application of microwave technologies will increase processes efficiency.</description><subject>Applied sciences</subject><subject>Chemical engineering</subject><subject>Crystallites</subject><subject>Drying</subject><subject>Evaporation</subject><subject>Exact sciences and technology</subject><subject>Hydrochlorides</subject><subject>Inclusion</subject><subject>Mechanical milling</subject><subject>Microwave irradiation</subject><subject>Microwaves</subject><subject>Milling</subject><subject>Miscellaneous</subject><subject>Precipitation</subject><subject>Solid-solid systems</subject><subject>Supersaturation</subject><issn>0032-5910</issn><issn>1873-328X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp9kE9LAzEQxYMoWKvfwEMugpetk2R3m14EEf-B4EXBW4jJxKakm5psq_vtTa149DTD8ObNvB8hpwwmDFh7sZis4mePZsLhZzQBJvfIiMmpqASXr_tkBCB41cwYHJKjnBcA0AoGI-IfOhfW2Bmk0dGlNyl-6g3S4jbvYojvA40dNdHo9Ba_hqAz0vlgUzTzEJO3SFc69d4EpNZvMGXfD1R3lto0-O6donPe-OI_HJMDp0PGk986Ji-3N8_X99Xj093D9dVjZUQ76yuOLXLrZCu4aGo9Y1pIZ3VjeKNbLjgAAjRcWlvz9k1iySSkEbY2UE9t6cbkfOe7SvFjjblXS58NhqA7jOusGHA-g2mxKNJ6Jy2pc07o1Cr5pU5DEaktWbVQO7JqS3Y7LWTL2tnvBZ2NDi7pzvj8t8uFrLcvFt3lTocl7sZjUvkHBVqf0PTKRv__oW-af5K2</recordid><startdate>20110215</startdate><enddate>20110215</enddate><creator>Pinchukova, Natalia A.</creator><creator>Chebanov, Valentin A.</creator><creator>Danilina, Viktoria V.</creator><creator>Desenko, Sergey M.</creator><creator>Seminozhenko, Volodymyr P.</creator><creator>Shishkin, Oleg V.</creator><creator>Voloshko, Alexander Yu</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20110215</creationdate><title>Influence of microwave technology on cocarboxylase hydrochloride particle diversity and drying efficiency</title><author>Pinchukova, Natalia A. ; Chebanov, Valentin A. ; Danilina, Viktoria V. ; Desenko, Sergey M. ; Seminozhenko, Volodymyr P. ; Shishkin, Oleg V. ; Voloshko, Alexander Yu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c369t-2e6e2df8632354a91a38fda5c25a623200e00528dd426b8e59138c3d4c047d8c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Applied sciences</topic><topic>Chemical engineering</topic><topic>Crystallites</topic><topic>Drying</topic><topic>Evaporation</topic><topic>Exact sciences and technology</topic><topic>Hydrochlorides</topic><topic>Inclusion</topic><topic>Mechanical milling</topic><topic>Microwave irradiation</topic><topic>Microwaves</topic><topic>Milling</topic><topic>Miscellaneous</topic><topic>Precipitation</topic><topic>Solid-solid systems</topic><topic>Supersaturation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Pinchukova, Natalia A.</creatorcontrib><creatorcontrib>Chebanov, Valentin A.</creatorcontrib><creatorcontrib>Danilina, Viktoria V.</creatorcontrib><creatorcontrib>Desenko, Sergey M.</creatorcontrib><creatorcontrib>Seminozhenko, Volodymyr P.</creatorcontrib><creatorcontrib>Shishkin, Oleg V.</creatorcontrib><creatorcontrib>Voloshko, Alexander Yu</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Powder technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Pinchukova, Natalia A.</au><au>Chebanov, Valentin A.</au><au>Danilina, Viktoria V.</au><au>Desenko, Sergey M.</au><au>Seminozhenko, Volodymyr P.</au><au>Shishkin, Oleg V.</au><au>Voloshko, Alexander Yu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of microwave technology on cocarboxylase hydrochloride particle diversity and drying efficiency</atitle><jtitle>Powder technology</jtitle><date>2011-02-15</date><risdate>2011</risdate><volume>207</volume><issue>1-3</issue><spage>134</spage><epage>139</epage><pages>134-139</pages><issn>0032-5910</issn><eissn>1873-328X</eissn><coden>POTEBX</coden><abstract>Two possible ways of crystallite downsizing of cocarboxylase hydrochloride namely mechanical milling and precipitation under high supersaturation conditions were studied as well as their influence on the drying parameters of the produced powders. It was found that both methods allowed shortening drying times of powders. However, precipitation from highly supersaturated solutions was found to have a more significant effect on cocarboxylase hydrochloride drying in comparison with the milling as the crystallites produced by the former method have smaller sizes (<10μm) without additional disintegration and contain much less inclusions of mother liquor. Obtaining solutions with high supersaturation degrees was achieved due to application of microwave irradiation at the evaporation stage that provided uniform gradientless heating of cocarboxylase aqueous solutions. The results of this work can be applied for producing other fine-crystalline substances and materials when particle sizes play a key role in the manufacture of products with the desired qualitative characteristics.
Drying times of cocarboxylase hydrochloride powders have been shown to be strongly dependant on particle diversity. Both mechanical milling of the powders obtained via uncontrollable crystallization and precipitation from highly supersaturated aqueous solutions have resulted in fine powders and considerable drying time shortening, the latter technique, however, demonstrated much more striking effect. [Display omitted]
► Microwave-assisted evaporation resulted in highly supersaturated solutions. ► Precipitation from highly supersaturated solutions resulted in very fine powders. ► Obtaining very fine powders allowed drying acceleration by the factor of 7. ► Application of microwave technologies will increase processes efficiency.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.powtec.2010.10.018</doi><tpages>6</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Applied sciences Chemical engineering Crystallites Drying Evaporation Exact sciences and technology Hydrochlorides Inclusion Mechanical milling Microwave irradiation Microwaves Milling Miscellaneous Precipitation Solid-solid systems Supersaturation |
| title | Influence of microwave technology on cocarboxylase hydrochloride particle diversity and drying efficiency |
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