Uncatalyzed synthesis of thiomorpholide using polyethylene glycol as green reaction media

Uncatalyzed synthesis of thiomorpholide using polyethylene glycol as green reaction media

Polyethylene glycol-600 was used as an efficient and recyclable solvent for the one-pot three component condensation reactions of aryl alkyl ketones, sulfur, and morpholine to produce the corresponding thiomorpholide. This protocol has advantages of high yields, short reaction times, mild reaction c...

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Veröffentlicht in:Green chemistry letters and reviews 2010-12, Vol.3 (4), p.315-318
Hauptverfasser: Gawande, Shrikant S., Bandgar, Babasaheb P., Kadam, Prasad D., Sable, Shailesh S.
Format: Artikel
Sprache:eng
Schlagworte:
Green chemistry
Immunoassay
Polyethylene glycol
polyethylene glycol-600
Polymers
sulfur
thiomorpholide
Willgerodt-Kindler reaction
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Zusammenfassung:Polyethylene glycol-600 was used as an efficient and recyclable solvent for the one-pot three component condensation reactions of aryl alkyl ketones, sulfur, and morpholine to produce the corresponding thiomorpholide. This protocol has advantages of high yields, short reaction times, mild reaction conditions, minimal environmental pollution, and simple work up procedure.
ISSN:1751-8253
1751-7192
DOI:10.1080/17518253.2010.486772