Investigating the Structural and Physicochemical Properties of Vicia ervilia Protein Isolate/Launaea acanthodes Gum Nanocomposite Film Containing Graphene Oxide Nanoparticles and Silybum marianum Extract Microcapsules

This study was conducted to generate and investigate the structural characteristics and antioxidant properties of a nano-composite film produced from Vicia ervilia protein (VEPI)— Launaea acanthodes gum (LAG). The film containing Silybum marianum extract microcapsules (SMEM) at varying volumes (0, 2...

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Veröffentlicht in:Journal of polymers and the environment 2024-09, Vol.32 (9), p.4661-4682
Hauptverfasser: Saray Tarkasheh, Sozhin, Alizadeh, Mohammad, Amiri, Saber, Karimi Sani, Iraj
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container_title Journal of polymers and the environment
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creator Saray Tarkasheh, Sozhin
Alizadeh, Mohammad
Amiri, Saber
Karimi Sani, Iraj
description This study was conducted to generate and investigate the structural characteristics and antioxidant properties of a nano-composite film produced from Vicia ervilia protein (VEPI)— Launaea acanthodes gum (LAG). The film containing Silybum marianum extract microcapsules (SMEM) at varying volumes (0, 2.2, 7.5, 12.8, 15 v/v) along with different concentrations of graphene oxide nanoparticles (GONPs) (0, 0.6, 2.0, 3.4, 4.0 w/v). The thickness, solubility, and moisture content of the film samples increased after the integration of SMEM and GONPs ( P  
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The film containing Silybum marianum extract microcapsules (SMEM) at varying volumes (0, 2.2, 7.5, 12.8, 15 v/v) along with different concentrations of graphene oxide nanoparticles (GONPs) (0, 0.6, 2.0, 3.4, 4.0 w/v). The thickness, solubility, and moisture content of the film samples increased after the integration of SMEM and GONPs ( P  &lt; 0.05). Fourier-transform infrared analysis of the film sample based on VEPI/LAG/SMEM/GONPs showed proper interactions, including electrostatic interaction between these materials. X-ray diffraction analysis revealed a lower degree of crystallinity in the nano-composite film by adding GONPs and SMEM. The Differential scanning calorimetry analysis conducted on the composite and optimized films, integrating SMEM and GONPs, revealed an elevation in both the glass transition temperature and the thermal degradation temperature compared to the blank sample. The results obtained from Field emission scanning electron microscopy demonstrated that the type and quantity of variables significantly influenced the surface morphology of the films, leading to the formation of cracks and pores in the film. Furthermore, the findings regarding antimicrobial activity demonstrated that the nanocomposite film, incorporating SMEM and GONPs, exhibited antimicrobial properties against E. coli and S. aureus bacteria. 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The results obtained from Field emission scanning electron microscopy demonstrated that the type and quantity of variables significantly influenced the surface morphology of the films, leading to the formation of cracks and pores in the film. Furthermore, the findings regarding antimicrobial activity demonstrated that the nanocomposite film, incorporating SMEM and GONPs, exhibited antimicrobial properties against E. coli and S. aureus bacteria. 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subjects Antimicrobial activity
Antimicrobial agents
Calorimetry
Chemistry
Chemistry and Materials Science
Degree of crystallinity
Differential scanning calorimetry
E coli
Electrostatic properties
Environmental Chemistry
Environmental Engineering/Biotechnology
Field emission microscopy
Food packaging
Fourier transforms
Glass transition temperature
Graphene
Industrial Chemistry/Chemical Engineering
Infrared analysis
Launaea
Materials Science
Microcapsules
Moisture content
Nanocomposites
Nanoparticles
Original Paper
Physicochemical properties
Polymer Sciences
Proteins
Scanning electron microscopy
Shelf life
Silybum marianum
Thermal degradation
Thickness
Transition temperatures
Vicia ervilia
Water content
X-ray diffraction
title Investigating the Structural and Physicochemical Properties of Vicia ervilia Protein Isolate/Launaea acanthodes Gum Nanocomposite Film Containing Graphene Oxide Nanoparticles and Silybum marianum Extract Microcapsules
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