Synthesis and characterization of BaGdTiFeO6: unveiling the microstructural, dielectric, and optical properties of a novel double perovskite
The novel double perovskite oxide material, BaGdTiFeO 6 (BGTFO), was synthesized using the solid-state reaction method. The material structure symmetry, morphology, and optical properties were investigated using a variety of techniques. XRD measurements showed that this material crystallizes in a cu...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2024-06, Vol.35 (17), p.1187, Article 1187 |
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| creator | Boudad, L. El Boukili, A. Taibi, M. Belayachi, A. Abd-lefdil, M. |
| description | The novel double perovskite oxide material, BaGdTiFeO
6
(BGTFO), was synthesized using the solid-state reaction method. The material structure symmetry, morphology, and optical properties were investigated using a variety of techniques. XRD measurements showed that this material crystallizes in a cubic double perovskite structure with a
P
m
3
¯
m
space group. The unit cell parameters, atomic positions, crystallite size, and site occupancies were determined using the Rietveld refinement method. Vibrational modes and bond deformations in the sample were examined through FTIR spectroscopy. Scanning electron microscopy revealed irregularly shaped grains with a non-uniform size distribution. The energy-dispersive X-ray spectroscopy (EDX) analysis confirmed the homogeneity, stoichiometry, and chemical formula of this double perovskite oxide. UV–Visible spectroscopy was employed to analyze the material’s absorbance, determining an energy bandgap of 2.05 eV. Additionally, the refractive index of the material was determined using both the Moss as well as the Herve and Vandamme methods, highlighting its potential for use in various application fields, including the optoelectronic industry. The interplay between frequency and temperature in influencing both the dielectric and conductivity characteristics of materials has also been investigated. |
| doi_str_mv | 10.1007/s10854-024-12983-w |
| format | Article |
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6
(BGTFO), was synthesized using the solid-state reaction method. The material structure symmetry, morphology, and optical properties were investigated using a variety of techniques. XRD measurements showed that this material crystallizes in a cubic double perovskite structure with a
P
m
3
¯
m
space group. The unit cell parameters, atomic positions, crystallite size, and site occupancies were determined using the Rietveld refinement method. Vibrational modes and bond deformations in the sample were examined through FTIR spectroscopy. Scanning electron microscopy revealed irregularly shaped grains with a non-uniform size distribution. The energy-dispersive X-ray spectroscopy (EDX) analysis confirmed the homogeneity, stoichiometry, and chemical formula of this double perovskite oxide. UV–Visible spectroscopy was employed to analyze the material’s absorbance, determining an energy bandgap of 2.05 eV. Additionally, the refractive index of the material was determined using both the Moss as well as the Herve and Vandamme methods, highlighting its potential for use in various application fields, including the optoelectronic industry. The interplay between frequency and temperature in influencing both the dielectric and conductivity characteristics of materials has also been investigated.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-024-12983-w</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Crystallites ; Energy distribution ; Homogeneity ; Materials Science ; Optical and Electronic Materials ; Optical properties ; Optoelectronics ; Perovskite structure ; Perovskites ; Refractivity ; Rietveld method ; Size distribution ; Spectroscopic analysis ; Spectrum analysis ; Stoichiometry ; Unit cell ; Vibration mode</subject><ispartof>Journal of materials science. Materials in electronics, 2024-06, Vol.35 (17), p.1187, Article 1187</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-c5316f9f9c4c76e130968138e425c9e083d08e574e5970a8a076ea551e4ba5483</cites><orcidid>0000-0001-9000-9110</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-024-12983-w$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-024-12983-w$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Boudad, L.</creatorcontrib><creatorcontrib>El Boukili, A.</creatorcontrib><creatorcontrib>Taibi, M.</creatorcontrib><creatorcontrib>Belayachi, A.</creatorcontrib><creatorcontrib>Abd-lefdil, M.</creatorcontrib><title>Synthesis and characterization of BaGdTiFeO6: unveiling the microstructural, dielectric, and optical properties of a novel double perovskite</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>The novel double perovskite oxide material, BaGdTiFeO
6
(BGTFO), was synthesized using the solid-state reaction method. The material structure symmetry, morphology, and optical properties were investigated using a variety of techniques. XRD measurements showed that this material crystallizes in a cubic double perovskite structure with a
P
m
3
¯
m
space group. The unit cell parameters, atomic positions, crystallite size, and site occupancies were determined using the Rietveld refinement method. Vibrational modes and bond deformations in the sample were examined through FTIR spectroscopy. Scanning electron microscopy revealed irregularly shaped grains with a non-uniform size distribution. The energy-dispersive X-ray spectroscopy (EDX) analysis confirmed the homogeneity, stoichiometry, and chemical formula of this double perovskite oxide. UV–Visible spectroscopy was employed to analyze the material’s absorbance, determining an energy bandgap of 2.05 eV. Additionally, the refractive index of the material was determined using both the Moss as well as the Herve and Vandamme methods, highlighting its potential for use in various application fields, including the optoelectronic industry. The interplay between frequency and temperature in influencing both the dielectric and conductivity characteristics of materials has also been investigated.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Crystallites</subject><subject>Energy distribution</subject><subject>Homogeneity</subject><subject>Materials Science</subject><subject>Optical and Electronic Materials</subject><subject>Optical properties</subject><subject>Optoelectronics</subject><subject>Perovskite structure</subject><subject>Perovskites</subject><subject>Refractivity</subject><subject>Rietveld method</subject><subject>Size distribution</subject><subject>Spectroscopic analysis</subject><subject>Spectrum analysis</subject><subject>Stoichiometry</subject><subject>Unit cell</subject><subject>Vibration mode</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9kMtO5DAQRS00SPQ0_AArS7MlQ_mVOLNj0NAgIbEAJHaWcSpgCHFjO43gG_ho3DTS7Fh5Ueeecl1C9hn8ZgDNYWKglayAy4rxVovqZYvMmGpEJTW_-UFm0KqmkorzHfIzpQcAqKXQM_J--Trme0w-UTt21N3baF3G6N9s9mGkoad_7aK78id4Uf-h07hCP_jxjpYQffIuhpTj5PIU7XBAO48Duhy9O_jUhWX2zg50GcMSY_aY1kJLx7DCgXZhuh2QlklYpUefcZds93ZIuPf1zsn1yb-r49Pq_GJxdnx0XjneQK6cEqzu27510jU1MgFtrZnQKLlyLYIWHWhUjUTVNmC1hUJZpRjKW6ukFnPya-Mt_3qeMGXzEKY4lpVGQAOMKeBtofiGWh-ZIvZmGf2Tja-GgVm3bjatm9K6-WzdvJSQ2IRSgcc7jP_V36Q-APs6h70</recordid><startdate>20240601</startdate><enddate>20240601</enddate><creator>Boudad, L.</creator><creator>El Boukili, A.</creator><creator>Taibi, M.</creator><creator>Belayachi, A.</creator><creator>Abd-lefdil, M.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0001-9000-9110</orcidid></search><sort><creationdate>20240601</creationdate><title>Synthesis and characterization of BaGdTiFeO6: unveiling the microstructural, dielectric, and optical properties of a novel double perovskite</title><author>Boudad, L. ; El Boukili, A. ; Taibi, M. ; Belayachi, A. ; Abd-lefdil, M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-c5316f9f9c4c76e130968138e425c9e083d08e574e5970a8a076ea551e4ba5483</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Crystallites</topic><topic>Energy distribution</topic><topic>Homogeneity</topic><topic>Materials Science</topic><topic>Optical and Electronic Materials</topic><topic>Optical properties</topic><topic>Optoelectronics</topic><topic>Perovskite structure</topic><topic>Perovskites</topic><topic>Refractivity</topic><topic>Rietveld method</topic><topic>Size distribution</topic><topic>Spectroscopic analysis</topic><topic>Spectrum analysis</topic><topic>Stoichiometry</topic><topic>Unit cell</topic><topic>Vibration mode</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Boudad, L.</creatorcontrib><creatorcontrib>El Boukili, A.</creatorcontrib><creatorcontrib>Taibi, M.</creatorcontrib><creatorcontrib>Belayachi, A.</creatorcontrib><creatorcontrib>Abd-lefdil, M.</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Boudad, L.</au><au>El Boukili, A.</au><au>Taibi, M.</au><au>Belayachi, A.</au><au>Abd-lefdil, M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of BaGdTiFeO6: unveiling the microstructural, dielectric, and optical properties of a novel double perovskite</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2024-06-01</date><risdate>2024</risdate><volume>35</volume><issue>17</issue><spage>1187</spage><pages>1187-</pages><artnum>1187</artnum><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>The novel double perovskite oxide material, BaGdTiFeO
6
(BGTFO), was synthesized using the solid-state reaction method. The material structure symmetry, morphology, and optical properties were investigated using a variety of techniques. XRD measurements showed that this material crystallizes in a cubic double perovskite structure with a
P
m
3
¯
m
space group. The unit cell parameters, atomic positions, crystallite size, and site occupancies were determined using the Rietveld refinement method. Vibrational modes and bond deformations in the sample were examined through FTIR spectroscopy. Scanning electron microscopy revealed irregularly shaped grains with a non-uniform size distribution. The energy-dispersive X-ray spectroscopy (EDX) analysis confirmed the homogeneity, stoichiometry, and chemical formula of this double perovskite oxide. UV–Visible spectroscopy was employed to analyze the material’s absorbance, determining an energy bandgap of 2.05 eV. Additionally, the refractive index of the material was determined using both the Moss as well as the Herve and Vandamme methods, highlighting its potential for use in various application fields, including the optoelectronic industry. The interplay between frequency and temperature in influencing both the dielectric and conductivity characteristics of materials has also been investigated.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-024-12983-w</doi><orcidid>https://orcid.org/0000-0001-9000-9110</orcidid></addata></record> |
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| ispartof | Journal of materials science. Materials in electronics, 2024-06, Vol.35 (17), p.1187, Article 1187 |
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| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Crystallites Energy distribution Homogeneity Materials Science Optical and Electronic Materials Optical properties Optoelectronics Perovskite structure Perovskites Refractivity Rietveld method Size distribution Spectroscopic analysis Spectrum analysis Stoichiometry Unit cell Vibration mode |
| title | Synthesis and characterization of BaGdTiFeO6: unveiling the microstructural, dielectric, and optical properties of a novel double perovskite |
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