The effect of chemical vapor infiltration process parameters on flexural strength of porous α$\alpha$‐SiC: a numerical model

The flexural strength variability of α$\alpha$‐SiC$\text{SiC}$ based ceramics at elevated temperatures creates the need for an Integrated Computational Materials Engineering (ICME) framework that relates the strength of a specimen directly to its manufacturing process. To create this ICME framework,...

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Veröffentlicht in:Journal of the American Ceramic Society 2024-07, Vol.107 (7), p.4604-4620
Hauptverfasser: Marziale, Joseph J., Sun, Jason, Walker, Eric A., Chen, Yu, Salac, David, Chen, James
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Sprache:eng
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Zusammenfassung:The flexural strength variability of α$\alpha$‐SiC$\text{SiC}$ based ceramics at elevated temperatures creates the need for an Integrated Computational Materials Engineering (ICME) framework that relates the strength of a specimen directly to its manufacturing process. To create this ICME framework, a model must first be developed which establishes a relationship between the chemical vapor infiltration (CVI) process and parameters, the resulting mesoscale pores, and the overall macroscale flexural strength. Here, a nonlinear single‐pore model of CVI is developed used in conjunction with a four‐way coupled thermo‐mechanical damage model. The individual components of the model are tested and a sample system under a four‐point bending test is explored. Results indicate that specimens with an initial porosity greater than 30% require temperatures below 1273 K to maintain structural integrity, while those with initial porosities less than 30% are temperature‐independent, allowing for optimization of the CVI processing time without compromising strength.
ISSN:0002-7820
1551-2916
DOI:10.1111/jace.19739