Synthesis, Structure, and Properties of Rhodium(II) Acetate Complexes with 2H-Azirines
Complexes of rhodium(II) acetate with 2 H -azirines were obtained for the first time. The 1 : 2 complexes were characterized using 1 H and 13 C NMR, IR, and UV spectroscopy and high-resolution mass spectrometry. The structure of Rh 2 (OAc) 4 complex with two 3-(4-methoxyphenyl)-2 H -azirine molecule...
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| Veröffentlicht in: | Russian journal of general chemistry 2024, Vol.94 (Suppl 1), p.S47-S52 |
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| container_issue | Suppl 1 |
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| container_title | Russian journal of general chemistry |
| container_volume | 94 |
| creator | Grishin, A. V. Filippov, I. P. Rostovskii, N. V. |
| description | Complexes of rhodium(II) acetate with 2
H
-azirines were obtained for the first time. The 1 : 2 complexes were characterized using
1
H and
13
C NMR, IR, and UV spectroscopy and high-resolution mass spectrometry. The structure of Rh
2
(OAc)
4
complex with two 3-(4-methoxyphenyl)-2
H
-azirine molecules was studied by X-ray diffraction analysis. In crystal, the molecule of this complex belongs to the C
i
point group. |
| doi_str_mv | 10.1134/S107036322414007X |
| format | Article |
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H
-azirines were obtained for the first time. The 1 : 2 complexes were characterized using
1
H and
13
C NMR, IR, and UV spectroscopy and high-resolution mass spectrometry. The structure of Rh
2
(OAc)
4
complex with two 3-(4-methoxyphenyl)-2
H
-azirine molecules was studied by X-ray diffraction analysis. In crystal, the molecule of this complex belongs to the C
i
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H
-azirines were obtained for the first time. The 1 : 2 complexes were characterized using
1
H and
13
C NMR, IR, and UV spectroscopy and high-resolution mass spectrometry. The structure of Rh
2
(OAc)
4
complex with two 3-(4-methoxyphenyl)-2
H
-azirine molecules was studied by X-ray diffraction analysis. In crystal, the molecule of this complex belongs to the C
i
point group.</description><subject>Acetates</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Heterocyclic compounds</subject><subject>Infrared spectroscopy</subject><subject>Mass spectrometry</subject><subject>Nitrogen</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Rhodium</subject><issn>1070-3632</issn><issn>1608-3350</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp1kFFLwzAUhYsoOKc_wLeCLwrrTJq0aR_LUDcYKE7Ft5KmN1tkbWqSovPXm1HBB5E83OTe890cThCcYzTFmNDrFUYMkZTEMcUUIfZ6EIxwirKIkAQd-rsfR_v5cXBi7RtCGKE0HgUvq13rNmCVnYQrZ3rhegOTkLd1-GB0B8YpsKGW4eNG16pvLheLq7AQ4LiDcKabbgufXvCh3CaM51HxpYxqwZ4GR5JvLZz91HHwfHvzNJtHy_u7xaxYRoIg5iLA3nQlJKWySgHRPMn8S9Z5xVPJcpkJWWWAKc_TJGcSZ1VcC8kE51kCtOZkHFwMezuj33uwrnzTvWn9l2WcM4Ip9SF41XRQrfkWStVK7QwX_tTQKKFbkMr3C5ax2IfCqAfwAAijrTUgy86ohptdiVG5z7v8k7dn4oGxXtuuwfxa-R_6BtqBgcI</recordid><startdate>2024</startdate><enddate>2024</enddate><creator>Grishin, A. V.</creator><creator>Filippov, I. P.</creator><creator>Rostovskii, N. V.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>2024</creationdate><title>Synthesis, Structure, and Properties of Rhodium(II) Acetate Complexes with 2H-Azirines</title><author>Grishin, A. V. ; Filippov, I. P. ; Rostovskii, N. V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c307t-e1703bcf44fb6e04958bcffd9ba6f79f8cfb8e14a96597f18b2dcf7caa85e4da3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Acetates</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Heterocyclic compounds</topic><topic>Infrared spectroscopy</topic><topic>Mass spectrometry</topic><topic>Nitrogen</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Rhodium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Grishin, A. V.</creatorcontrib><creatorcontrib>Filippov, I. P.</creatorcontrib><creatorcontrib>Rostovskii, N. V.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of general chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Grishin, A. V.</au><au>Filippov, I. P.</au><au>Rostovskii, N. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis, Structure, and Properties of Rhodium(II) Acetate Complexes with 2H-Azirines</atitle><jtitle>Russian journal of general chemistry</jtitle><stitle>Russ J Gen Chem</stitle><date>2024</date><risdate>2024</risdate><volume>94</volume><issue>Suppl 1</issue><spage>S47</spage><epage>S52</epage><pages>S47-S52</pages><issn>1070-3632</issn><eissn>1608-3350</eissn><abstract>Complexes of rhodium(II) acetate with 2
H
-azirines were obtained for the first time. The 1 : 2 complexes were characterized using
1
H and
13
C NMR, IR, and UV spectroscopy and high-resolution mass spectrometry. The structure of Rh
2
(OAc)
4
complex with two 3-(4-methoxyphenyl)-2
H
-azirine molecules was studied by X-ray diffraction analysis. In crystal, the molecule of this complex belongs to the C
i
point group.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S107036322414007X</doi></addata></record> |
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| issn | 1070-3632 1608-3350 |
| language | eng |
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| subjects | Acetates Chemistry Chemistry and Materials Science Chemistry/Food Science Heterocyclic compounds Infrared spectroscopy Mass spectrometry Nitrogen NMR Nuclear magnetic resonance Rhodium |
| title | Synthesis, Structure, and Properties of Rhodium(II) Acetate Complexes with 2H-Azirines |
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