Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization
In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra- n -butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution sys...
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Veröffentlicht in: | Polymer bulletin (Berlin, Germany) Germany), 2015-04, Vol.72 (4), p.867-879 |
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creator | Bolat, Gulcin Kuralay, Filiz Temelli, Baris Unaleroglu, Canan Abaci, Serdar |
description | In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra-
n
-butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques. |
doi_str_mv | 10.1007/s00289-015-1311-x |
format | Article |
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n
-butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques.</description><identifier>ISSN: 0170-0839</identifier><identifier>EISSN: 1436-2449</identifier><identifier>DOI: 10.1007/s00289-015-1311-x</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Acids ; Ammonium perchlorates ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Complex Fluids and Microfluidics ; Dichloromethane ; Electrochemical analysis ; Electrochemistry ; Electrodes ; Electrolytes ; Fourier transforms ; Microscopy ; Morphology ; NMR ; NMR spectroscopy ; Nuclear magnetic resonance ; Organic Chemistry ; Original Paper ; Oxidation ; Physical Chemistry ; Polymer films ; Polymer Sciences ; Polymerization ; Polymers ; Scanning electron microscopy ; Soft and Granular Matter ; Spectrum analysis ; Voltammetry</subject><ispartof>Polymer bulletin (Berlin, Germany), 2015-04, Vol.72 (4), p.867-879</ispartof><rights>Springer-Verlag Berlin Heidelberg 2015</rights><rights>Springer-Verlag Berlin Heidelberg 2015.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c423t-ea46e7f07287cca9a67de268aaf3536a2e4555e54bb041462802ab77d488d59a3</citedby><cites>FETCH-LOGICAL-c423t-ea46e7f07287cca9a67de268aaf3536a2e4555e54bb041462802ab77d488d59a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00289-015-1311-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2918070737?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21386,27922,27923,33742,41486,42555,43803,51317,64383,64387,72239</link.rule.ids></links><search><creatorcontrib>Bolat, Gulcin</creatorcontrib><creatorcontrib>Kuralay, Filiz</creatorcontrib><creatorcontrib>Temelli, Baris</creatorcontrib><creatorcontrib>Unaleroglu, Canan</creatorcontrib><creatorcontrib>Abaci, Serdar</creatorcontrib><title>Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization</title><title>Polymer bulletin (Berlin, Germany)</title><addtitle>Polym. Bull</addtitle><description>In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra-
n
-butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques.</description><subject>Acids</subject><subject>Ammonium perchlorates</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Complex Fluids and Microfluidics</subject><subject>Dichloromethane</subject><subject>Electrochemical analysis</subject><subject>Electrochemistry</subject><subject>Electrodes</subject><subject>Electrolytes</subject><subject>Fourier transforms</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>NMR</subject><subject>NMR spectroscopy</subject><subject>Nuclear magnetic resonance</subject><subject>Organic Chemistry</subject><subject>Original Paper</subject><subject>Oxidation</subject><subject>Physical Chemistry</subject><subject>Polymer films</subject><subject>Polymer Sciences</subject><subject>Polymerization</subject><subject>Polymers</subject><subject>Scanning electron microscopy</subject><subject>Soft and Granular Matter</subject><subject>Spectrum analysis</subject><subject>Voltammetry</subject><issn>0170-0839</issn><issn>1436-2449</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kEtLxDAUhYMoOI7-AHcFN7qI3rzTpQw-GXCj65BJU9thpqlJBqb-ejtUcOXqcuB858KH0CWBWwKg7hIA1SUGIjBhhOD9EZoRziSmnJfHaAZEAQbNylN0ltIaxiwlmaHXh413OQbX-G2bchyKUBd92AzXAveN74ZNUbX9EGPY-tzYzt8UtquKNqfCNTZal31sv21uQ3eOTmq7Sf7i987Rx-PD--IZL9-eXhb3S-w4ZRl7y6VXNSiqlXO2tFJVnkptbc0Ek5Z6LoTwgq9WwAmXVAO1K6UqrnUlSsvm6Gra7WP42vmUzTrsYje-NLQkGhQopsYWmVouhpSir00f262NgyFgDsrMpMyMysxBmdmPDJ2YNHa7Tx__lv-HfgC6V282</recordid><startdate>20150401</startdate><enddate>20150401</enddate><creator>Bolat, Gulcin</creator><creator>Kuralay, Filiz</creator><creator>Temelli, Baris</creator><creator>Unaleroglu, Canan</creator><creator>Abaci, Serdar</creator><general>Springer Berlin Heidelberg</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope></search><sort><creationdate>20150401</creationdate><title>Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization</title><author>Bolat, Gulcin ; Kuralay, Filiz ; Temelli, Baris ; Unaleroglu, Canan ; Abaci, Serdar</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c423t-ea46e7f07287cca9a67de268aaf3536a2e4555e54bb041462802ab77d488d59a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Acids</topic><topic>Ammonium perchlorates</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Complex Fluids and Microfluidics</topic><topic>Dichloromethane</topic><topic>Electrochemical analysis</topic><topic>Electrochemistry</topic><topic>Electrodes</topic><topic>Electrolytes</topic><topic>Fourier transforms</topic><topic>Microscopy</topic><topic>Morphology</topic><topic>NMR</topic><topic>NMR spectroscopy</topic><topic>Nuclear magnetic resonance</topic><topic>Organic Chemistry</topic><topic>Original Paper</topic><topic>Oxidation</topic><topic>Physical Chemistry</topic><topic>Polymer films</topic><topic>Polymer Sciences</topic><topic>Polymerization</topic><topic>Polymers</topic><topic>Scanning electron microscopy</topic><topic>Soft and Granular Matter</topic><topic>Spectrum analysis</topic><topic>Voltammetry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bolat, Gulcin</creatorcontrib><creatorcontrib>Kuralay, Filiz</creatorcontrib><creatorcontrib>Temelli, Baris</creatorcontrib><creatorcontrib>Unaleroglu, Canan</creatorcontrib><creatorcontrib>Abaci, Serdar</creatorcontrib><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection (ProQuest)</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><jtitle>Polymer bulletin (Berlin, Germany)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bolat, Gulcin</au><au>Kuralay, Filiz</au><au>Temelli, Baris</au><au>Unaleroglu, Canan</au><au>Abaci, Serdar</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization</atitle><jtitle>Polymer bulletin (Berlin, Germany)</jtitle><stitle>Polym. Bull</stitle><date>2015-04-01</date><risdate>2015</risdate><volume>72</volume><issue>4</issue><spage>867</spage><epage>879</epage><pages>867-879</pages><issn>0170-0839</issn><eissn>1436-2449</eissn><abstract>In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra-
n
-butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s00289-015-1311-x</doi><tpages>13</tpages></addata></record> |
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subjects | Acids Ammonium perchlorates Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Complex Fluids and Microfluidics Dichloromethane Electrochemical analysis Electrochemistry Electrodes Electrolytes Fourier transforms Microscopy Morphology NMR NMR spectroscopy Nuclear magnetic resonance Organic Chemistry Original Paper Oxidation Physical Chemistry Polymer films Polymer Sciences Polymerization Polymers Scanning electron microscopy Soft and Granular Matter Spectrum analysis Voltammetry |
title | Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization |
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