Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization

In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra- n -butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution sys...

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Veröffentlicht in:	Polymer bulletin (Berlin, Germany) Germany), 2015-04, Vol.72 (4), p.867-879
Hauptverfasser:	Bolat, Gulcin, Kuralay, Filiz, Temelli, Baris, Unaleroglu, Canan, Abaci, Serdar
Format:	Artikel
Sprache:	eng
Schlagworte:	Acids Ammonium perchlorates Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Complex Fluids and Microfluidics Dichloromethane Electrochemical analysis Electrochemistry Electrodes Electrolytes Fourier transforms Microscopy Morphology NMR NMR spectroscopy Nuclear magnetic resonance Organic Chemistry Original Paper Oxidation Physical Chemistry Polymer films Polymer Sciences Polymerization Polymers Scanning electron microscopy Soft and Granular Matter Spectrum analysis Voltammetry
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Beschreibung
Zusammenfassung:	In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra- n -butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques.
ISSN:	0170-0839 1436-2449
DOI:	10.1007/s00289-015-1311-x