Effect of Coating Stoichiometry and Annealing on Phase Composition of Y–Al–O Compounds

The paper presents research results of Y–Al–O system-based coatings synthesized by cathodic-arc deposition simultaneously from two electric-arc evaporators with single-component Y and Al cathodes. Three different modes of annealing are used. After the deposition process, the coatings are annealed in...

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Veröffentlicht in:Russian physics journal 2023-03, Vol.65 (11), p.1908-1916
Hauptverfasser: Nazarov, A. Yu, Khusainova, A. M., Maslov, A. A., Ramazanov, K. N., Syrtanov, M. S., Nikolaev, A. A., Tulina, A. A., Vardanyan, E. L.
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container_end_page 1916
container_issue 11
container_start_page 1908
container_title Russian physics journal
container_volume 65
creator Nazarov, A. Yu
Khusainova, A. M.
Maslov, A. A.
Ramazanov, K. N.
Syrtanov, M. S.
Nikolaev, A. A.
Tulina, A. A.
Vardanyan, E. L.
description The paper presents research results of Y–Al–O system-based coatings synthesized by cathodic-arc deposition simultaneously from two electric-arc evaporators with single-component Y and Al cathodes. Three different modes of annealing are used. After the deposition process, the coatings are annealed in a vacuum furnace at 800 and at 1200°C to identify the effect from the annealing temperature on the phase composition. The formation of the YAlO 3 phase occurs in all annealing modes. More complex Y 3 Al 5 O 12 and Y 4 Al 2 O 9 oxides appear with increasing process temperature. According to the X-ray diffraction analysis, the process temperature and deposition mode affect the phase composition of the coating, which acquires the amorphous structure. The coating structure is studied on a scanning electron microscope. After 1200°C annealing, the coating sublayer diffusion occurs in the base material.
doi_str_mv 10.1007/s11182-023-02850-2
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According to the X-ray diffraction analysis, the process temperature and deposition mode affect the phase composition of the coating, which acquires the amorphous structure. The coating structure is studied on a scanning electron microscope. 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subjects Analysis
Annealing
Annealing furnaces
Arc deposition
Cathodic coating (process)
Coating effects
Coatings
Condensed Matter Physics
Diffraction
Diffusion coating
Evaporators
Furnaces
Hadrons
Heavy Ions
Lasers
Mathematical and Computational Physics
Nuclear Physics
Optical Devices
Optics
Phase composition
Photonics
Physics
Physics and Astronomy
Stoichiometry
Theoretical
Vacuum furnaces
X-rays
title Effect of Coating Stoichiometry and Annealing on Phase Composition of Y–Al–O Compounds
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