Study on Sintering Behavior of Reaction-Cured Glass Coating
High-emissivity coatings constitute an essential component of reusable thermal protection systems, determining the success or failure of hypersonic spacecraft. Reaction-cured glass coating is the basis for all current high-emissivity coatings, and the study of its sintering behavior is of great scie...
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| Veröffentlicht in: | Coatings (Basel) 2023-02, Vol.13 (2), p.463 |
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| creator | Li, Mingwei Sun, Yulei Zeng, Gang Li, Wenhao Zhong, Yesheng Shi, Liping Wang, Rongguo He, Xiaodong |
| description | High-emissivity coatings constitute an essential component of reusable thermal protection systems, determining the success or failure of hypersonic spacecraft. Reaction-cured glass coating is the basis for all current high-emissivity coatings, and the study of its sintering behavior is of great scientific significance for the development and performance enhancement of the coating. Microstructures and phase compositions of the samples before and after the sintering process were determined using SEM, XRD, and EDS. The sintering temperature, inserting temperature, and heating rate were systematically investigated. The results show that the effects of the sintering temperature, inserting temperature, and heating rate on the coating occur in decreasing order. The optimum condition for coating sintering in this study is an insertion temperature of 1100 °C, a heating rate of 10 °C/min, and a sintering temperature of 1200 °C, and a crack-free and containing SiB4 borosilicate glass coating was successfully prepared. |
| doi_str_mv | 10.3390/coatings13020463 |
| format | Article |
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Reaction-cured glass coating is the basis for all current high-emissivity coatings, and the study of its sintering behavior is of great scientific significance for the development and performance enhancement of the coating. Microstructures and phase compositions of the samples before and after the sintering process were determined using SEM, XRD, and EDS. The sintering temperature, inserting temperature, and heating rate were systematically investigated. The results show that the effects of the sintering temperature, inserting temperature, and heating rate on the coating occur in decreasing order. The optimum condition for coating sintering in this study is an insertion temperature of 1100 °C, a heating rate of 10 °C/min, and a sintering temperature of 1200 °C, and a crack-free and containing SiB4 borosilicate glass coating was successfully prepared.</description><identifier>ISSN: 2079-6412</identifier><identifier>EISSN: 2079-6412</identifier><identifier>DOI: 10.3390/coatings13020463</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Borosilicate glass ; Coatings ; Electronic equipment and supplies ; Emissivity ; Glass coatings ; Heat ; Heating rate ; Morphology ; Phase composition ; Radiation ; Reusable spacecraft ; Sintering ; Spectrum analysis ; Thermal protection</subject><ispartof>Coatings (Basel), 2023-02, Vol.13 (2), p.463</ispartof><rights>COPYRIGHT 2023 MDPI AG</rights><rights>2023 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). 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The optimum condition for coating sintering in this study is an insertion temperature of 1100 °C, a heating rate of 10 °C/min, and a sintering temperature of 1200 °C, and a crack-free and containing SiB4 borosilicate glass coating was successfully prepared.</description><subject>Borosilicate glass</subject><subject>Coatings</subject><subject>Electronic equipment and supplies</subject><subject>Emissivity</subject><subject>Glass coatings</subject><subject>Heat</subject><subject>Heating rate</subject><subject>Morphology</subject><subject>Phase composition</subject><subject>Radiation</subject><subject>Reusable spacecraft</subject><subject>Sintering</subject><subject>Spectrum analysis</subject><subject>Thermal protection</subject><issn>2079-6412</issn><issn>2079-6412</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdUM9LwzAUDqLgmLt7LHjuTPKSpsHTLDqFgeD0XNIknRldM5NW2H9vpB7E9w7v8fh-PD6ErgleAkh8q70aXL-LBDDFrIAzNKNYyLxghJ7_2S_RIsY9TiUJlETO0N12GM0p8322df1gQ1LJ7u2H-nI-ZL7NXq3Sg_N9Xo3BmmzdqRizarK7Qhet6qJd_M45en98eKue8s3L-rlabXINmA-5LLklpRStoI2A0jQEGtEUTAHnFEvaNLwgJr2kCgAFJdVgmSGgGQPNjYE5upl0j8F_jjYO9d6PoU-WNRVCcioIgYRaTqid6mzt-tYPQenUxh6c9r1tXbqvBANMKCcsEfBE0MHHGGxbH4M7qHCqCa5_Yq3_xwrfHvpp7w</recordid><startdate>20230201</startdate><enddate>20230201</enddate><creator>Li, Mingwei</creator><creator>Sun, Yulei</creator><creator>Zeng, Gang</creator><creator>Li, Wenhao</creator><creator>Zhong, Yesheng</creator><creator>Shi, Liping</creator><creator>Wang, Rongguo</creator><creator>He, Xiaodong</creator><general>MDPI AG</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><orcidid>https://orcid.org/0000-0003-1151-9302</orcidid></search><sort><creationdate>20230201</creationdate><title>Study on Sintering Behavior of Reaction-Cured Glass Coating</title><author>Li, Mingwei ; 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Reaction-cured glass coating is the basis for all current high-emissivity coatings, and the study of its sintering behavior is of great scientific significance for the development and performance enhancement of the coating. Microstructures and phase compositions of the samples before and after the sintering process were determined using SEM, XRD, and EDS. The sintering temperature, inserting temperature, and heating rate were systematically investigated. The results show that the effects of the sintering temperature, inserting temperature, and heating rate on the coating occur in decreasing order. 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| source | MDPI - Multidisciplinary Digital Publishing Institute; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection |
| subjects | Borosilicate glass Coatings Electronic equipment and supplies Emissivity Glass coatings Heat Heating rate Morphology Phase composition Radiation Reusable spacecraft Sintering Spectrum analysis Thermal protection |
| title | Study on Sintering Behavior of Reaction-Cured Glass Coating |
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