Homemade Silver/Silver chloride ink with low curing temperature for screen-printed electrodes
[Display omitted] •A simple procedure is presented for the low temperature curing Ag/AgCl ink synthesis;•The ink has interesting features like low resistivity and high conductivity;•The good performance of the ink in reference electrode from a flexible SPE was successful illustrated for the electroc...
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Veröffentlicht in: | Journal of electroanalytical chemistry (Lausanne, Switzerland) Switzerland), 2022-06, Vol.915, p.116316, Article 116316 |
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Sprache: | eng |
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•A simple procedure is presented for the low temperature curing Ag/AgCl ink synthesis;•The ink has interesting features like low resistivity and high conductivity;•The good performance of the ink in reference electrode from a flexible SPE was successful illustrated for the electrochemical detection of carbendazim.
Here we report the synthesis of Ag/AgCl ink with low curing temperature for application in electrochemical sensors. The ink characterization was carried out by atomic force microscopy, scanning electron microscopy with energy dispersive spectroscopy, X-ray diffraction, thermogravimetry analysis, DC electrical resistivity, and cyclic voltammetry. Furthermore, the ink was used in a pseudo reference electrode of a screen-printed device, which was then applied for carbendazim quantification as proof of concept. The electrochemical sensor presented linear response in the range of carbendazim concentrations from 0.25 to 1.48 µmol L−1 and limit of detection of 0.10 µmol L−1, suggesting the potential of the as-developed ink for designing miniaturized electrochemical sensing devices. |
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ISSN: | 1572-6657 1873-2569 |
DOI: | 10.1016/j.jelechem.2022.116316 |