Synthesis and Thermal Transformations of Nickel(II) Salts of Saturated Monocarboxylic Acid—Precursors of Metal-Containing Nanocomposites

Nickel(II) salts are synthesized with saturated monocarboxylic acids: butyric, valeric, caproic, enanthic, and caprylic. The resulting compounds are characterized by elemental analysis, infrared (IR) spectroscopy, and differential scanning calorimetry. As a result of thermal decomposition of the syn...

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Veröffentlicht in:	Nanobiotechnology Reports (Online) 2022-06, Vol.17 (3), p.345-355
Hauptverfasser:	Saprykin, R. V., Semenov, S. A., Drobot, D. V., Volchkova, E. V., Dzhardimalieva, G. I., Ivanova, A. I., Golovanov, A. B., Popenko, V. I.
Format:	Artikel
Sprache:	eng
Schlagworte:	Carboxylates Chemistry and Materials Science Differential scanning calorimetry Functional and Construction Nanomaterials Industrial and Production Engineering Infrared analysis Infrared spectroscopy Machines Magnetic properties Manufacturing Materials Science Nanocomposites Nanotechnology Nickel Processes Spectroscopic analysis Synthesis Thermal decomposition Thermal transformations X-ray spectroscopy
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Zusammenfassung:	Nickel(II) salts are synthesized with saturated monocarboxylic acids: butyric, valeric, caproic, enanthic, and caprylic. The resulting compounds are characterized by elemental analysis, infrared (IR) spectroscopy, and differential scanning calorimetry. As a result of thermal decomposition of the synthesized carboxylates, nickel-containing nanocomposites are obtained, which are studied by scanning and transmission electron microscopy, elemental analysis, IR spectroscopy, energy-dispersive X-ray spectroscopy, and X-ray phase analysis. The magnetic properties of the obtained nanocomposites are studied.
ISSN:	2635-1676 1995-0780 2635-1684 1995-0799
DOI:	10.1134/S2635167622030156