Synthesis of bulk superconductors using the sol-gel method
In this study, High temperature superconductor YBa2Cu3O7-x (YBCO) nanoparticle was prepared by Sol-gel technique. The sol-gel includes a homogeneous solution of Y-Ba-Cu acetate precursor and acetic acid. The powder was compressed by hydraulic at 5 ton/cm2 and needed a post-reaction heat treatment at...
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| creator | Hussein, Amir A. Abdul Hasan, N. Hussein, Adi M. Abdul Mohammed, Faras Q. |
| description | In this study, High temperature superconductor YBa2Cu3O7-x (YBCO) nanoparticle was prepared by Sol-gel technique. The sol-gel includes a homogeneous solution of Y-Ba-Cu acetate precursor and acetic acid. The powder was compressed by hydraulic at 5 ton/cm2 and needed a post-reaction heat treatment at 850 °C for 8 h with oxygen flow. The YBCO bulk has been characterized using traditional R-T measurements, producing a best value of the critical transition temperature (Tc) of approximately 93 °k. The morphology of the samples taken by scanning electron microscopy (SEM) views particles after heating processing, as well as the best Nano scale and clearly plate shaped grains. Furthermore, the EDX revealed that the composition of elements YBCO matched the chemicals used to make the YBCO superconductor. X-Ray Diffraction (XRD) was used to examine the structural properties of the Y-123 compound, which revealed that the sample is crystalline with an orthorhombic phase. |
| doi_str_mv | 10.1063/5.0108818 |
| format | Conference Proceeding |
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Abdul ; Hasan, N. ; Hussein, Adi M. Abdul ; Mohammed, Faras Q.</creator><contributor>Salame, Chafic-Touma ; Shaban, Auday ; Aillerie, Michel ; Jabur, Akram R.</contributor><creatorcontrib>Hussein, Amir A. Abdul ; Hasan, N. ; Hussein, Adi M. Abdul ; Mohammed, Faras Q. ; Salame, Chafic-Touma ; Shaban, Auday ; Aillerie, Michel ; Jabur, Akram R.</creatorcontrib><description>In this study, High temperature superconductor YBa2Cu3O7-x (YBCO) nanoparticle was prepared by Sol-gel technique. The sol-gel includes a homogeneous solution of Y-Ba-Cu acetate precursor and acetic acid. The powder was compressed by hydraulic at 5 ton/cm2 and needed a post-reaction heat treatment at 850 °C for 8 h with oxygen flow. The YBCO bulk has been characterized using traditional R-T measurements, producing a best value of the critical transition temperature (Tc) of approximately 93 °k. The morphology of the samples taken by scanning electron microscopy (SEM) views particles after heating processing, as well as the best Nano scale and clearly plate shaped grains. Furthermore, the EDX revealed that the composition of elements YBCO matched the chemicals used to make the YBCO superconductor. X-Ray Diffraction (XRD) was used to examine the structural properties of the Y-123 compound, which revealed that the sample is crystalline with an orthorhombic phase.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/5.0108818</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Acetic acid ; Heat treatment ; High temperature superconductors ; Nanoparticles ; Orthorhombic phase ; Sol-gel processes ; Transition temperature ; YBCO superconductors</subject><ispartof>AIP conference proceedings, 2022, Vol.2437 (1)</ispartof><rights>Author(s)</rights><rights>2022 Author(s). 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Abdul</creatorcontrib><creatorcontrib>Mohammed, Faras Q.</creatorcontrib><title>Synthesis of bulk superconductors using the sol-gel method</title><title>AIP conference proceedings</title><description>In this study, High temperature superconductor YBa2Cu3O7-x (YBCO) nanoparticle was prepared by Sol-gel technique. The sol-gel includes a homogeneous solution of Y-Ba-Cu acetate precursor and acetic acid. The powder was compressed by hydraulic at 5 ton/cm2 and needed a post-reaction heat treatment at 850 °C for 8 h with oxygen flow. The YBCO bulk has been characterized using traditional R-T measurements, producing a best value of the critical transition temperature (Tc) of approximately 93 °k. The morphology of the samples taken by scanning electron microscopy (SEM) views particles after heating processing, as well as the best Nano scale and clearly plate shaped grains. Furthermore, the EDX revealed that the composition of elements YBCO matched the chemicals used to make the YBCO superconductor. X-Ray Diffraction (XRD) was used to examine the structural properties of the Y-123 compound, which revealed that the sample is crystalline with an orthorhombic phase.</description><subject>Acetic acid</subject><subject>Heat treatment</subject><subject>High temperature superconductors</subject><subject>Nanoparticles</subject><subject>Orthorhombic phase</subject><subject>Sol-gel processes</subject><subject>Transition temperature</subject><subject>YBCO superconductors</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2022</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp9kM9LwzAYhoMoOKcH_4OAN6Hz-5qkSbzJ8BcMPLiDt9CmydbZNTVphf33Tjbw5um9PO_7wkPINcIMoWB3YgYISqE6IRMUAjNZYHFKJgCaZzlnH-fkIqUNQK6lVBNy_77rhrVLTaLB02psP2kaexdt6OrRDiEmOqamW9E9RFNos5Vr6dYN61BfkjNftsldHXNKlk-Py_lLtnh7fp0_LLJeK5-5EjmvSs6EtlZ5sFZXkldc5t4DA196yYTPc115LSruWa0kKpC1sAxBMDYlN4fZPoav0aXBbMIYu_2jySUwFMgLvaduD1SyzVAOTehMH5ttGXfmO0QjzFGL6Wv_H4xgfj3-FdgP8VBkCQ</recordid><startdate>20220817</startdate><enddate>20220817</enddate><creator>Hussein, Amir A. Abdul</creator><creator>Hasan, N.</creator><creator>Hussein, Adi M. Abdul</creator><creator>Mohammed, Faras Q.</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20220817</creationdate><title>Synthesis of bulk superconductors using the sol-gel method</title><author>Hussein, Amir A. Abdul ; Hasan, N. ; Hussein, Adi M. Abdul ; Mohammed, Faras Q.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p98f-ea144ba4359cc8f0cc9b74b472ff030faf735f229bf95b4f3d871807d5c310533</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Acetic acid</topic><topic>Heat treatment</topic><topic>High temperature superconductors</topic><topic>Nanoparticles</topic><topic>Orthorhombic phase</topic><topic>Sol-gel processes</topic><topic>Transition temperature</topic><topic>YBCO superconductors</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hussein, Amir A. Abdul</creatorcontrib><creatorcontrib>Hasan, N.</creatorcontrib><creatorcontrib>Hussein, Adi M. 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Abdul</au><au>Mohammed, Faras Q.</au><au>Salame, Chafic-Touma</au><au>Shaban, Auday</au><au>Aillerie, Michel</au><au>Jabur, Akram R.</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Synthesis of bulk superconductors using the sol-gel method</atitle><btitle>AIP conference proceedings</btitle><date>2022-08-17</date><risdate>2022</risdate><volume>2437</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>In this study, High temperature superconductor YBa2Cu3O7-x (YBCO) nanoparticle was prepared by Sol-gel technique. The sol-gel includes a homogeneous solution of Y-Ba-Cu acetate precursor and acetic acid. The powder was compressed by hydraulic at 5 ton/cm2 and needed a post-reaction heat treatment at 850 °C for 8 h with oxygen flow. The YBCO bulk has been characterized using traditional R-T measurements, producing a best value of the critical transition temperature (Tc) of approximately 93 °k. The morphology of the samples taken by scanning electron microscopy (SEM) views particles after heating processing, as well as the best Nano scale and clearly plate shaped grains. Furthermore, the EDX revealed that the composition of elements YBCO matched the chemicals used to make the YBCO superconductor. X-Ray Diffraction (XRD) was used to examine the structural properties of the Y-123 compound, which revealed that the sample is crystalline with an orthorhombic phase.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/5.0108818</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0094-243X |
| ispartof | AIP conference proceedings, 2022, Vol.2437 (1) |
| issn | 0094-243X 1551-7616 |
| language | eng |
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| source | AIP Journals Complete |
| subjects | Acetic acid Heat treatment High temperature superconductors Nanoparticles Orthorhombic phase Sol-gel processes Transition temperature YBCO superconductors |
| title | Synthesis of bulk superconductors using the sol-gel method |
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