Peculiarities of the Spectral Characteristics of Brassinosteroids of the 24-Epibrassinolide and 6-deoxo-24-epitheasterone Series in NMR Spectra in Deuteropyridine and Deuterochloroform

Peculiarities of the Spectral Characteristics of Brassinosteroids of the 24-Epibrassinolide and 6-deoxo-24-epitheasterone Series in NMR Spectra in Deuteropyridine and Deuterochloroform

Resonances of hydrogen and carbon nuclei in steroids belonging to the 6-deoxo-24-epitheasterone and 24-epibrassinolide classes were assigned using two-dimensional nuclear magnetic resonance spectroscopy. Solvent effects on the chemical shifts were studied.

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Veröffentlicht in:Journal of applied spectroscopy 2022-05, Vol.89 (2), p.218-224
Hauptverfasser: Baranovsky, A. V., Aver’kova, M. A., Litvinovskaya, R. P.
Format: Artikel
Sprache:eng
Schlagworte:
Alfacalcidol
Analytical Chemistry
Atomic/Molecular Structure and Spectra
Calcifediol
Hydrogen
NMR spectroscopy
Nuclear magnetic resonance spectroscopy
Physics
Physics and Astronomy
Solvent effect
Steroids
Vitamin D
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Zusammenfassung:Resonances of hydrogen and carbon nuclei in steroids belonging to the 6-deoxo-24-epitheasterone and 24-epibrassinolide classes were assigned using two-dimensional nuclear magnetic resonance spectroscopy. Solvent effects on the chemical shifts were studied.
ISSN:0021-9037
1573-8647
DOI:10.1007/s10812-022-01346-0