Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones
2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via C -acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N , N -dimethylaminopyridine in acetonitrile at room temperature. Structure of the syn...
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| Veröffentlicht in: | Russian journal of general chemistry 2021-08, Vol.91 (8), p.1438-1443 |
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| container_title | Russian journal of general chemistry |
| container_volume | 91 |
| creator | Khlebnicova, T. S. Zinovich, V. G. Piven, Yu. A. Baranovsky, A. V. Lakhvich, F. A. Trifonov, R. E. |
| description | 2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via
C
-acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and
N
,
N
-dimethylaminopyridine in acetonitrile at room temperature. Structure of the synthesized compounds was confirmed by
1
H,
13
C NMR spectroscopy, as well as two-dimensional NMR spectroscopy methods. |
| doi_str_mv | 10.1134/S1070363221080028 |
| format | Article |
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C
-acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and
N
,
N
-dimethylaminopyridine in acetonitrile at room temperature. Structure of the synthesized compounds was confirmed by
1
H,
13
C NMR spectroscopy, as well as two-dimensional NMR spectroscopy methods.</description><identifier>ISSN: 1070-3632</identifier><identifier>EISSN: 1608-3350</identifier><identifier>DOI: 10.1134/S1070363221080028</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Acetonitrile ; Acylation ; Antibiotics ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Cyclohexane ; Diketones ; Ethyldimethylaminopropyl carbodiimide ; NMR spectroscopy ; Nuclear magnetic resonance spectroscopy ; Plant metabolites ; Room temperature ; Spectrum analysis ; Synthesis</subject><ispartof>Russian journal of general chemistry, 2021-08, Vol.91 (8), p.1438-1443</ispartof><rights>Pleiades Publishing, Ltd. 2021</rights><rights>COPYRIGHT 2021 Springer</rights><rights>Pleiades Publishing, Ltd. 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c383t-4fcbdede3d6353cb9137209963e58d61167b5615ff304a144b4a74fc16d7eec43</citedby><cites>FETCH-LOGICAL-c383t-4fcbdede3d6353cb9137209963e58d61167b5615ff304a144b4a74fc16d7eec43</cites><orcidid>0000-0003-0023-6534 ; 0000-0001-9295-3279 ; 0000-0003-3640-0981 ; 0000-0003-3463-4936</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1070363221080028$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1070363221080028$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Khlebnicova, T. S.</creatorcontrib><creatorcontrib>Zinovich, V. G.</creatorcontrib><creatorcontrib>Piven, Yu. A.</creatorcontrib><creatorcontrib>Baranovsky, A. V.</creatorcontrib><creatorcontrib>Lakhvich, F. A.</creatorcontrib><creatorcontrib>Trifonov, R. E.</creatorcontrib><title>Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones</title><title>Russian journal of general chemistry</title><addtitle>Russ J Gen Chem</addtitle><description>2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via
C
-acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and
N
,
N
-dimethylaminopyridine in acetonitrile at room temperature. Structure of the synthesized compounds was confirmed by
1
H,
13
C NMR spectroscopy, as well as two-dimensional NMR spectroscopy methods.</description><subject>Acetonitrile</subject><subject>Acylation</subject><subject>Antibiotics</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Cyclohexane</subject><subject>Diketones</subject><subject>Ethyldimethylaminopropyl carbodiimide</subject><subject>NMR spectroscopy</subject><subject>Nuclear magnetic resonance spectroscopy</subject><subject>Plant metabolites</subject><subject>Room temperature</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><issn>1070-3632</issn><issn>1608-3350</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp1kE1Lw0AQhhdRsFZ_gLeCFwVTdzKbTXIsxS8QPLSel2Qz26ak2bqbgvHXu6VCEZU5zDDzPvPF2CXwMQCKuxnwlKPEOAaecR5nR2wAkmcRYsKPQxzK0a5-ys68X3EOnMt4wNJZ33ZL8rUfWTOKo-s5da74tE3fFJq6vrnRvW7skj6KliK4xaiqbUv-nJ2YovF08e2H7O3hfj59il5eH5-nk5dIY4ZdJIwuK6oIK4kJ6jIHTGOe5xIpySoJINMykZAYg1wUIEQpijRAIKuUSAscsqt9342z71vynVrZrWvDSBUnKQeRBOigWhQNqbo1Nhyh17XXapJChjnITAbV-A9VsIrWtQ5XmTrkfwCwB7Sz3jsyauPqdeF6BVzt3q5-vT0w8Z7xQdsuyB0W_h_6AmqEgEk</recordid><startdate>20210801</startdate><enddate>20210801</enddate><creator>Khlebnicova, T. S.</creator><creator>Zinovich, V. G.</creator><creator>Piven, Yu. A.</creator><creator>Baranovsky, A. V.</creator><creator>Lakhvich, F. A.</creator><creator>Trifonov, R. E.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-0023-6534</orcidid><orcidid>https://orcid.org/0000-0001-9295-3279</orcidid><orcidid>https://orcid.org/0000-0003-3640-0981</orcidid><orcidid>https://orcid.org/0000-0003-3463-4936</orcidid></search><sort><creationdate>20210801</creationdate><title>Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones</title><author>Khlebnicova, T. S. ; Zinovich, V. G. ; Piven, Yu. A. ; Baranovsky, A. V. ; Lakhvich, F. A. ; Trifonov, R. E.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c383t-4fcbdede3d6353cb9137209963e58d61167b5615ff304a144b4a74fc16d7eec43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Acetonitrile</topic><topic>Acylation</topic><topic>Antibiotics</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Cyclohexane</topic><topic>Diketones</topic><topic>Ethyldimethylaminopropyl carbodiimide</topic><topic>NMR spectroscopy</topic><topic>Nuclear magnetic resonance spectroscopy</topic><topic>Plant metabolites</topic><topic>Room temperature</topic><topic>Spectrum analysis</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Khlebnicova, T. S.</creatorcontrib><creatorcontrib>Zinovich, V. G.</creatorcontrib><creatorcontrib>Piven, Yu. A.</creatorcontrib><creatorcontrib>Baranovsky, A. V.</creatorcontrib><creatorcontrib>Lakhvich, F. A.</creatorcontrib><creatorcontrib>Trifonov, R. E.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of general chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Khlebnicova, T. S.</au><au>Zinovich, V. G.</au><au>Piven, Yu. A.</au><au>Baranovsky, A. V.</au><au>Lakhvich, F. A.</au><au>Trifonov, R. E.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones</atitle><jtitle>Russian journal of general chemistry</jtitle><stitle>Russ J Gen Chem</stitle><date>2021-08-01</date><risdate>2021</risdate><volume>91</volume><issue>8</issue><spage>1438</spage><epage>1443</epage><pages>1438-1443</pages><issn>1070-3632</issn><eissn>1608-3350</eissn><abstract>2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via
C
-acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and
N
,
N
-dimethylaminopyridine in acetonitrile at room temperature. Structure of the synthesized compounds was confirmed by
1
H,
13
C NMR spectroscopy, as well as two-dimensional NMR spectroscopy methods.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1070363221080028</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0003-0023-6534</orcidid><orcidid>https://orcid.org/0000-0001-9295-3279</orcidid><orcidid>https://orcid.org/0000-0003-3640-0981</orcidid><orcidid>https://orcid.org/0000-0003-3463-4936</orcidid></addata></record> |
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| issn | 1070-3632 1608-3350 |
| language | eng |
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| source | SpringerNature Journals |
| subjects | Acetonitrile Acylation Antibiotics Chemistry Chemistry and Materials Science Chemistry/Food Science Cyclohexane Diketones Ethyldimethylaminopropyl carbodiimide NMR spectroscopy Nuclear magnetic resonance spectroscopy Plant metabolites Room temperature Spectrum analysis Synthesis |
| title | Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones |
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