Synthesis of 2-(Tetrazolylacetyl)cyclohexane-1,3-diones

2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via C -acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N , N -dimethylaminopyridine in acetonitrile at room temperature. Structure of the syn...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Veröffentlicht in:	Russian journal of general chemistry 2021-08, Vol.91 (8), p.1438-1443
Hauptverfasser:	Khlebnicova, T. S., Zinovich, V. G., Piven, Yu. A., Baranovsky, A. V., Lakhvich, F. A., Trifonov, R. E.
Format:	Artikel
Sprache:	eng
Schlagworte:	Acetonitrile Acylation Antibiotics Chemistry Chemistry and Materials Science Chemistry/Food Science Cyclohexane Diketones Ethyldimethylaminopropyl carbodiimide NMR spectroscopy Nuclear magnetic resonance spectroscopy Plant metabolites Room temperature Spectrum analysis Synthesis
Online-Zugang:	Volltext
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	2-(Tetrazolylacetyl)cyclohexane-1,3-diones were synthesized via C -acylation of cyclohexane-1,3-diones with tetrazolylacetic acids in the presence of 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N , N -dimethylaminopyridine in acetonitrile at room temperature. Structure of the synthesized compounds was confirmed by 1 H, 13 C NMR spectroscopy, as well as two-dimensional NMR spectroscopy methods.
ISSN:	1070-3632 1608-3350
DOI:	10.1134/S1070363221080028