Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties
The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been...
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creator | Nartu, M.S.K.K.Y. Dasari, S. Sharma, A. Mantri, S.A. Sharma, Shashank Pantawane, Mangesh V. McWilliams, B. Cho, K. Dahotre, Narendra B. Banerjee, R. |
description | The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been reported in conventionally processed counterparts. The large solidification range for this alloy resulted in finer scale equiaxed β grains in the as deposited condition for a range of process parameters, unlike the large columnar grains observed in case of AM of other titanium alloys such as Ti–6Al–4V. Furthermore, based on the process parameters, a homogeneous distribution of fine scale ω or α precipitates form within the β grains, which has been rationalized based on quantitative thermo-kinetic modelling of a multi-layered deposition process. Atom probe tomography results indicate early stages of β/ω compositional partitioning, leading to a higher tensile yield strength, close to 1000 MPa, as compared to the solution treated/quenched condition of conventionally processed Ti-185. Homogeneous fine scale α precipitation, with a more pronounced compositional partitioning, resulted in an exceptional yield strength exceeding 1200 MPa in the as-processed condition.
•A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters. |
doi_str_mv | 10.1016/j.msea.2021.141627 |
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•A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters.</description><identifier>ISSN: 0921-5093</identifier><identifier>EISSN: 1873-4936</identifier><identifier>DOI: 10.1016/j.msea.2021.141627</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Beta fleck effect ; Commercial beta titanium alloy ; Deposition ; Equiaxed grains ; High strength alloys ; Laser additive manufacturing ; LENS ; Mechanical properties ; Multilayers ; Partitioning ; Precipitates ; Process parameters ; Solidification ; Titanium alloys ; Titanium base alloys ; Yield strength ; Yield stress</subject><ispartof>Materials science & engineering. A, Structural materials : properties, microstructure and processing, 2021-07, Vol.821, p.141627, Article 141627</ispartof><rights>2021 Elsevier B.V.</rights><rights>Copyright Elsevier BV Jul 21, 2021</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c372t-78d715878865cc7f0c671f352a06285bead98779db6539c91314dcb3d08096d33</citedby><cites>FETCH-LOGICAL-c372t-78d715878865cc7f0c671f352a06285bead98779db6539c91314dcb3d08096d33</cites><orcidid>0000-0003-0527-0133 ; 0000-0003-4703-7030 ; 0000-0003-4165-5073 ; 0000-0001-5992-0299</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.msea.2021.141627$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids></links><search><creatorcontrib>Nartu, M.S.K.K.Y.</creatorcontrib><creatorcontrib>Dasari, S.</creatorcontrib><creatorcontrib>Sharma, A.</creatorcontrib><creatorcontrib>Mantri, S.A.</creatorcontrib><creatorcontrib>Sharma, Shashank</creatorcontrib><creatorcontrib>Pantawane, Mangesh V.</creatorcontrib><creatorcontrib>McWilliams, B.</creatorcontrib><creatorcontrib>Cho, K.</creatorcontrib><creatorcontrib>Dahotre, Narendra B.</creatorcontrib><creatorcontrib>Banerjee, R.</creatorcontrib><title>Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties</title><title>Materials science & engineering. A, Structural materials : properties, microstructure and processing</title><description>The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been reported in conventionally processed counterparts. The large solidification range for this alloy resulted in finer scale equiaxed β grains in the as deposited condition for a range of process parameters, unlike the large columnar grains observed in case of AM of other titanium alloys such as Ti–6Al–4V. Furthermore, based on the process parameters, a homogeneous distribution of fine scale ω or α precipitates form within the β grains, which has been rationalized based on quantitative thermo-kinetic modelling of a multi-layered deposition process. Atom probe tomography results indicate early stages of β/ω compositional partitioning, leading to a higher tensile yield strength, close to 1000 MPa, as compared to the solution treated/quenched condition of conventionally processed Ti-185. Homogeneous fine scale α precipitation, with a more pronounced compositional partitioning, resulted in an exceptional yield strength exceeding 1200 MPa in the as-processed condition.
•A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters.</description><subject>Beta fleck effect</subject><subject>Commercial beta titanium alloy</subject><subject>Deposition</subject><subject>Equiaxed grains</subject><subject>High strength alloys</subject><subject>Laser additive manufacturing</subject><subject>LENS</subject><subject>Mechanical properties</subject><subject>Multilayers</subject><subject>Partitioning</subject><subject>Precipitates</subject><subject>Process parameters</subject><subject>Solidification</subject><subject>Titanium alloys</subject><subject>Titanium base alloys</subject><subject>Yield strength</subject><subject>Yield stress</subject><issn>0921-5093</issn><issn>1873-4936</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNp9kUtuFDEQhi0EEkPCBVhZYt2DH-22W2ITRQSQImUTsrVq7Oppj_qF7R5pdtyBW3CsnCQehjWb8sL11Veqn5APnG05482nw3ZMCFvBBN_ymjdCvyIbbrSs6lY2r8mGtYJXirXyLXmX0oExxmumNuTPw4h7oEeMaU0UhqUHukR0YQkZcpgnOqIPkNHT3an8zA5TogtEGDEXiIaJgvchhyMOJzrCtHbg8hoL0Id9T1OOOO1zTx_D86_f_GYo1TyVou6w-Ib5RGHyNOQyalwKSv86XQ9TcDCclQvGHDBdkzcdDAnf_3uvyI-7L4-336r7h6_fb2_uKye1yJU2XnNltDGNck53zDWad1IJYI0waofgW6N163eNkq1rueS1dzvpmWFt46W8Ih8vc4v654op28O8xqkorVBNrYwUgpUucelycU4pYmeXGEaIJ8uZPWdiD_aciT1nYi-ZFOjzBcKy_zFgtMkFnFw5cbl5tn4O_8NfAP13mn8</recordid><startdate>20210721</startdate><enddate>20210721</enddate><creator>Nartu, M.S.K.K.Y.</creator><creator>Dasari, S.</creator><creator>Sharma, A.</creator><creator>Mantri, S.A.</creator><creator>Sharma, Shashank</creator><creator>Pantawane, Mangesh V.</creator><creator>McWilliams, B.</creator><creator>Cho, K.</creator><creator>Dahotre, Narendra B.</creator><creator>Banerjee, R.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0003-0527-0133</orcidid><orcidid>https://orcid.org/0000-0003-4703-7030</orcidid><orcidid>https://orcid.org/0000-0003-4165-5073</orcidid><orcidid>https://orcid.org/0000-0001-5992-0299</orcidid></search><sort><creationdate>20210721</creationdate><title>Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties</title><author>Nartu, M.S.K.K.Y. ; Dasari, S. ; Sharma, A. ; Mantri, S.A. ; Sharma, Shashank ; Pantawane, Mangesh V. ; McWilliams, B. ; Cho, K. ; Dahotre, Narendra B. ; Banerjee, R.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c372t-78d715878865cc7f0c671f352a06285bead98779db6539c91314dcb3d08096d33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Beta fleck effect</topic><topic>Commercial beta titanium alloy</topic><topic>Deposition</topic><topic>Equiaxed grains</topic><topic>High strength alloys</topic><topic>Laser additive manufacturing</topic><topic>LENS</topic><topic>Mechanical properties</topic><topic>Multilayers</topic><topic>Partitioning</topic><topic>Precipitates</topic><topic>Process parameters</topic><topic>Solidification</topic><topic>Titanium alloys</topic><topic>Titanium base alloys</topic><topic>Yield strength</topic><topic>Yield stress</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nartu, M.S.K.K.Y.</creatorcontrib><creatorcontrib>Dasari, S.</creatorcontrib><creatorcontrib>Sharma, A.</creatorcontrib><creatorcontrib>Mantri, S.A.</creatorcontrib><creatorcontrib>Sharma, Shashank</creatorcontrib><creatorcontrib>Pantawane, Mangesh V.</creatorcontrib><creatorcontrib>McWilliams, B.</creatorcontrib><creatorcontrib>Cho, K.</creatorcontrib><creatorcontrib>Dahotre, Narendra B.</creatorcontrib><creatorcontrib>Banerjee, R.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nartu, M.S.K.K.Y.</au><au>Dasari, S.</au><au>Sharma, A.</au><au>Mantri, S.A.</au><au>Sharma, Shashank</au><au>Pantawane, Mangesh V.</au><au>McWilliams, B.</au><au>Cho, K.</au><au>Dahotre, Narendra B.</au><au>Banerjee, R.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties</atitle><jtitle>Materials science & engineering. A, Structural materials : properties, microstructure and processing</jtitle><date>2021-07-21</date><risdate>2021</risdate><volume>821</volume><spage>141627</spage><pages>141627-</pages><artnum>141627</artnum><issn>0921-5093</issn><eissn>1873-4936</eissn><abstract>The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been reported in conventionally processed counterparts. The large solidification range for this alloy resulted in finer scale equiaxed β grains in the as deposited condition for a range of process parameters, unlike the large columnar grains observed in case of AM of other titanium alloys such as Ti–6Al–4V. Furthermore, based on the process parameters, a homogeneous distribution of fine scale ω or α precipitates form within the β grains, which has been rationalized based on quantitative thermo-kinetic modelling of a multi-layered deposition process. Atom probe tomography results indicate early stages of β/ω compositional partitioning, leading to a higher tensile yield strength, close to 1000 MPa, as compared to the solution treated/quenched condition of conventionally processed Ti-185. Homogeneous fine scale α precipitation, with a more pronounced compositional partitioning, resulted in an exceptional yield strength exceeding 1200 MPa in the as-processed condition.
•A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2021.141627</doi><orcidid>https://orcid.org/0000-0003-0527-0133</orcidid><orcidid>https://orcid.org/0000-0003-4703-7030</orcidid><orcidid>https://orcid.org/0000-0003-4165-5073</orcidid><orcidid>https://orcid.org/0000-0001-5992-0299</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Beta fleck effect Commercial beta titanium alloy Deposition Equiaxed grains High strength alloys Laser additive manufacturing LENS Mechanical properties Multilayers Partitioning Precipitates Process parameters Solidification Titanium alloys Titanium base alloys Yield strength Yield stress |
title | Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties |
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