Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties

The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been...

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Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2021-07, Vol.821, p.141627, Article 141627
Hauptverfasser: Nartu, M.S.K.K.Y., Dasari, S., Sharma, A., Mantri, S.A., Sharma, Shashank, Pantawane, Mangesh V., McWilliams, B., Cho, K., Dahotre, Narendra B., Banerjee, R.
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container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
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creator Nartu, M.S.K.K.Y.
Dasari, S.
Sharma, A.
Mantri, S.A.
Sharma, Shashank
Pantawane, Mangesh V.
McWilliams, B.
Cho, K.
Dahotre, Narendra B.
Banerjee, R.
description The high strength metastable β-Ti alloy, Ti–1Al–8V–5Fe (wt%), also referred to as Ti-185, has been successfully processed using the directed energy deposition (DED) based laser engineered net shaping (LENS) process, obviating the beta fleck problem associated with Fe micro-segregation that has been reported in conventionally processed counterparts. The large solidification range for this alloy resulted in finer scale equiaxed β grains in the as deposited condition for a range of process parameters, unlike the large columnar grains observed in case of AM of other titanium alloys such as Ti–6Al–4V. Furthermore, based on the process parameters, a homogeneous distribution of fine scale ω or α precipitates form within the β grains, which has been rationalized based on quantitative thermo-kinetic modelling of a multi-layered deposition process. Atom probe tomography results indicate early stages of β/ω compositional partitioning, leading to a higher tensile yield strength, close to 1000 MPa, as compared to the solution treated/quenched condition of conventionally processed Ti-185. Homogeneous fine scale α precipitation, with a more pronounced compositional partitioning, resulted in an exceptional yield strength exceeding 1200 MPa in the as-processed condition. •A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters.
doi_str_mv 10.1016/j.msea.2021.141627
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Furthermore, based on the process parameters, a homogeneous distribution of fine scale ω or α precipitates form within the β grains, which has been rationalized based on quantitative thermo-kinetic modelling of a multi-layered deposition process. Atom probe tomography results indicate early stages of β/ω compositional partitioning, leading to a higher tensile yield strength, close to 1000 MPa, as compared to the solution treated/quenched condition of conventionally processed Ti-185. Homogeneous fine scale α precipitation, with a more pronounced compositional partitioning, resulted in an exceptional yield strength exceeding 1200 MPa in the as-processed condition. •A commercial β Ti alloy prone to β flecking, Ti-185 has been successfully fabricated via LENS.•A higher laser power (500 W) resulted in ω precipitation within the equiaxed β grains.•A lower laser power (300 W) resulted in α precipitation within the equiaxed β grains.•Influence of laser power on α/ω precipitation, has been justified using multi-physics thermo-kinetic model.•Ability to tune the microstructure via changes in the process parameters.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.msea.2021.141627</doi><orcidid>https://orcid.org/0000-0003-0527-0133</orcidid><orcidid>https://orcid.org/0000-0003-4703-7030</orcidid><orcidid>https://orcid.org/0000-0003-4165-5073</orcidid><orcidid>https://orcid.org/0000-0001-5992-0299</orcidid><oa>free_for_read</oa></addata></record>
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source Elsevier ScienceDirect Journals
subjects Beta fleck effect
Commercial beta titanium alloy
Deposition
Equiaxed grains
High strength alloys
Laser additive manufacturing
LENS
Mechanical properties
Multilayers
Partitioning
Precipitates
Process parameters
Solidification
Titanium alloys
Titanium base alloys
Yield strength
Yield stress
title Omega versus alpha precipitation mediated by process parameters in additively manufactured high strength Ti–1Al–8V–5Fe alloy and its impact on mechanical properties
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