The application of vacuum redistillation of patchouli oil to improve patchouli alcohol compound

Patchouli oil produced by traditional distillation of patchouli leaves and stems by farmers in Aceh still has low patchouli alcohol compound. In order to increase patchouli alcohol concentration, vacuum redistillation process using packed column was introduced. This research was conducted to fractionate terpene (alpha-copinene) from oxygenated hydrocarbon (patchouli alcohol) compound. The operation condition was conducted at two variables that was dependent variable and independent variable. The dependent variable was the 30 cm height distillation packed column, by using raschig ring with 8 mm x 8 mm dimension. And the independent variable was operating temperature 130 °C and 140 °C., vacuum pressure 143,61 mbar, 121,60 mbar and 88,59 mbar and operation time 2 hours, 3 hours and 5 hours. Total of treatments applied in this works were 3 x 3 x 3 or equal to 27 treatments. Patchouli oil used in this research was obtained from Desa Teladan-Lembah Seulawah, Aceh Province. The initial patchouli alcohol compound which analyzed with GC-MS contained 16,02% before treatment applied. After vacuum redistillation process treatment applied patchouli oil concentration increase up to 34,67%. Physico-chemical test of patchouli oil after vacuum redistillation is in accordance with SNI 06-23852006 standard.