New Synthesis of 3,3′,3″-Nitrilotripropionic Acid

A new procedure has been developed for the synthesis of 3,3′,3″ - nitrilotripropionic acid (NTP) by reaction of formamide with acrylic acid in a solvent under pressure 100–130°C. The product structure was confirmed by IR and 1 H and 13 C NMR spectra, X-ray diffraction data, and elemental analysis....

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Veröffentlicht in:Russian journal of organic chemistry 2021-06, Vol.57 (6), p.1006-1008
Hauptverfasser: Lisin, A. V., Akhmadullin, R. M., Akhmadullina, A. G., Spiridonova, R. R.
Format: Artikel
Sprache:eng
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Zusammenfassung:A new procedure has been developed for the synthesis of 3,3′,3″ - nitrilotripropionic acid (NTP) by reaction of formamide with acrylic acid in a solvent under pressure 100–130°C. The product structure was confirmed by IR and 1 H and 13 C NMR spectra, X-ray diffraction data, and elemental analysis.
ISSN:1070-4280
1608-3393
DOI:10.1134/S107042802106018X