Synthesis of Imidoyl Chlorides Using Phosphorus Trichloride

Synthesis of Imidoyl Chlorides Using Phosphorus Trichloride

The reaction of carboxamides with phosphorus trichloride under heating at 75–80°C for 1 h in the presence of a 4-dimethylaminopyridine catalyst was used to synthesize imidoyl chlorides in yields of 63–99%.

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Veröffentlicht in:Russian journal of organic chemistry 2021-05, Vol.57 (5), p.849-851
Hauptverfasser: Shishkin, E. V., Vo, T. L. Q., Popov, Yu. V., Zotov, Yu. L., Nguyen, T. L., Shishkin, V. E.
Format: Artikel
Sprache:eng
Schlagworte:
Chemical synthesis
Chemistry
Chemistry and Materials Science
Chlorides
Organic Chemistry
Phosphorus
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Beschreibung
Zusammenfassung:The reaction of carboxamides with phosphorus trichloride under heating at 75–80°C for 1 h in the presence of a 4-dimethylaminopyridine catalyst was used to synthesize imidoyl chlorides in yields of 63–99%.
ISSN:1070-4280
1608-3393
DOI:10.1134/S1070428021050134