Real-time monitoring and control for high-efficiency autonomous laser fabrication of silicon nanoparticle colloids
Nanotechnology is a significant research tool for biological and medical research with major advancements achieved from nanoparticle (Np) applications in biosensing and biotherapeutics. For laser ablation synthesis in solution (LASiS) to be chosen by researchers for Np colloid production, the proces...
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| Veröffentlicht in: | International journal of advanced manufacturing technology 2021-05, Vol.114 (1-2), p.291-304 |
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| container_title | International journal of advanced manufacturing technology |
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| creator | Freeland, Brian McCann, Ronan O’Neill, Paul Sreenilayam, Sithara Tiefenthaler, Manuel Dabros, Michal Juillerat, Mandy Foley, Greg Brabazon, Dermot |
| description | Nanotechnology is a significant research tool for biological and medical research with major advancements achieved from nanoparticle (Np) applications in biosensing and biotherapeutics. For laser ablation synthesis in solution (LASiS) to be chosen by researchers for Np colloid production, the process must effectively compete with chemical synthesis in terms of produced colloid quality and productivity while taking advantage of LASiS benefits in terms of its ‘green-synthesis’ and single-step functionalisation abilities. In this work, a newly developed integrated LASiS Np manufacturing system is presented including a Np flow reactor design, an at-line Np size monitoring via 180° dynamic light scattering, and a UV-Vis spectroscopy system used to estimate colloid concentration and stability. The experimental outcomes are discussed in terms of Np productivity and quality via these at-line measurements from the UV-Vis and DLS systems. The developed instrument was validated via off-line SiNps DLS, UV-Vis and morphology tests via TEM. Ultra-high quality and nanoparticle fabrication rate efficiency was achieved and is reported here. |
| doi_str_mv | 10.1007/s00170-021-06772-6 |
| format | Article |
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For laser ablation synthesis in solution (LASiS) to be chosen by researchers for Np colloid production, the process must effectively compete with chemical synthesis in terms of produced colloid quality and productivity while taking advantage of LASiS benefits in terms of its ‘green-synthesis’ and single-step functionalisation abilities. In this work, a newly developed integrated LASiS Np manufacturing system is presented including a Np flow reactor design, an at-line Np size monitoring via 180° dynamic light scattering, and a UV-Vis spectroscopy system used to estimate colloid concentration and stability. The experimental outcomes are discussed in terms of Np productivity and quality via these at-line measurements from the UV-Vis and DLS systems. The developed instrument was validated via off-line SiNps DLS, UV-Vis and morphology tests via TEM. Ultra-high quality and nanoparticle fabrication rate efficiency was achieved and is reported here.</description><identifier>ISSN: 0268-3768</identifier><identifier>EISSN: 1433-3015</identifier><identifier>DOI: 10.1007/s00170-021-06772-6</identifier><language>eng</language><publisher>London: Springer London</publisher><subject>CAE) and Design ; Chemical synthesis ; Colloiding ; Computer-Aided Engineering (CAD ; Engineering ; Industrial and Production Engineering ; Laser ablation ; Mechanical Engineering ; Media Management ; Medical research ; Monitoring ; Morphology ; Nanoparticles ; Nanotechnology ; Original Article ; Photon correlation spectroscopy ; Productivity ; Reactor design</subject><ispartof>International journal of advanced manufacturing technology, 2021-05, Vol.114 (1-2), p.291-304</ispartof><rights>The Author(s), under exclusive licence to Springer-Verlag London Ltd. part of Springer Nature 2021</rights><rights>The Author(s), under exclusive licence to Springer-Verlag London Ltd. part of Springer Nature 2021.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-152e2da30f6e420a7114e6dfe4469a371cba35e6709e43f35b82452c0a5aab2d3</citedby><cites>FETCH-LOGICAL-c319t-152e2da30f6e420a7114e6dfe4469a371cba35e6709e43f35b82452c0a5aab2d3</cites><orcidid>0000-0002-2071-0785</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00170-021-06772-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00170-021-06772-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Freeland, Brian</creatorcontrib><creatorcontrib>McCann, Ronan</creatorcontrib><creatorcontrib>O’Neill, Paul</creatorcontrib><creatorcontrib>Sreenilayam, Sithara</creatorcontrib><creatorcontrib>Tiefenthaler, Manuel</creatorcontrib><creatorcontrib>Dabros, Michal</creatorcontrib><creatorcontrib>Juillerat, Mandy</creatorcontrib><creatorcontrib>Foley, Greg</creatorcontrib><creatorcontrib>Brabazon, Dermot</creatorcontrib><title>Real-time monitoring and control for high-efficiency autonomous laser fabrication of silicon nanoparticle colloids</title><title>International journal of advanced manufacturing technology</title><addtitle>Int J Adv Manuf Technol</addtitle><description>Nanotechnology is a significant research tool for biological and medical research with major advancements achieved from nanoparticle (Np) applications in biosensing and biotherapeutics. 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Ultra-high quality and nanoparticle fabrication rate efficiency was achieved and is reported here.</description><subject>CAE) and Design</subject><subject>Chemical synthesis</subject><subject>Colloiding</subject><subject>Computer-Aided Engineering (CAD</subject><subject>Engineering</subject><subject>Industrial and Production Engineering</subject><subject>Laser ablation</subject><subject>Mechanical Engineering</subject><subject>Media Management</subject><subject>Medical research</subject><subject>Monitoring</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Original Article</subject><subject>Photon correlation spectroscopy</subject><subject>Productivity</subject><subject>Reactor design</subject><issn>0268-3768</issn><issn>1433-3015</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kEtLxDAURoMoOI7-AVcB19E82qSzlMEXDAii63CbJjMZ2mRM0sX8e6sV3Lm6m--cCweha0ZvGaXqLlPKFCWUM0KlUpzIE7RglRBEUFafogXlsiFCyeYcXeS8n-aSyWaB0puFnhQ_WDzE4EtMPmwxhA6bGEqKPXYx4Z3f7oh1zhtvgzliGEsMcYhjxj1km7CDNnkDxceAo8PZ937icYAQD5CKN72dhH0ffZcv0ZmDPtur37tEH48P7-tnsnl9elnfb4gRbFUIq7nlHQjqpK04BcVYZWXnbFXJFQjFTAuitlLRla2EE3Xb8KrmhkIN0PJOLNHN7D2k-DnaXPQ-jilMLzWvGReNknU1rfi8MinmnKzTh-QHSEfNqP5uq-e2emqrf9pqOUFihvLhu5dNf-p_qC_kQ352</recordid><startdate>20210501</startdate><enddate>20210501</enddate><creator>Freeland, Brian</creator><creator>McCann, Ronan</creator><creator>O’Neill, Paul</creator><creator>Sreenilayam, Sithara</creator><creator>Tiefenthaler, Manuel</creator><creator>Dabros, Michal</creator><creator>Juillerat, Mandy</creator><creator>Foley, Greg</creator><creator>Brabazon, Dermot</creator><general>Springer London</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M7S</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0002-2071-0785</orcidid></search><sort><creationdate>20210501</creationdate><title>Real-time monitoring and control for high-efficiency autonomous laser fabrication of silicon nanoparticle colloids</title><author>Freeland, Brian ; 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| subjects | CAE) and Design Chemical synthesis Colloiding Computer-Aided Engineering (CAD Engineering Industrial and Production Engineering Laser ablation Mechanical Engineering Media Management Medical research Monitoring Morphology Nanoparticles Nanotechnology Original Article Photon correlation spectroscopy Productivity Reactor design |
| title | Real-time monitoring and control for high-efficiency autonomous laser fabrication of silicon nanoparticle colloids |
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