Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT)
In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revea...
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Veröffentlicht in: | International journal of refractory metals & hard materials 2020-08, Vol.90, p.105234, Article 105234 |
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Sprache: | eng |
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Zusammenfassung: | In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revealed a uniform dispersion of the Nb additives in the diamond matrix and no interfacial cracking was observed. Higher concentration of binder increased tendency to intergranular failure. The formation of NbC and NbC0.84 phases after sintering was identified, indicating that some of the matrix carbon may have undergone graphitization.
•Niobium at different concentrations was introduced as a binder for the PCD.•High integrity samples were prepared via HPHT route.•NbC and NbC0.84 phase formation was observed at diamond interfaces after sintering.•Metallic matrix increased young's modulus and tendency to intergranular failure. |
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ISSN: | 0263-4368 2213-3917 |
DOI: | 10.1016/j.ijrmhm.2020.105234 |