Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT)

In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revea...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:International journal of refractory metals & hard materials 2020-08, Vol.90, p.105234, Article 105234
Hauptverfasser: Gurgel, Diego Pires, Rodrigues, Mayara Adrielly Leal de Oliveira, Mashhadikarimi, Meysam, Barreto, Lucas Pires de Paiva, Filgueira, Marcello, Bichler, Lukas, Gomes, Uílame Umbelino
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:In this research, the effect of adding 2.5, 5.0 and 10 wt% niobium (Nb) as a binding agent was investigated for High Pressure-High Temperature (HPHT) sintering of polycrystalline diamond (PCD). Samples were sintered at 1750 °C and 7.7 GPa. Detailed characterization of the as-sintered materials revealed a uniform dispersion of the Nb additives in the diamond matrix and no interfacial cracking was observed. Higher concentration of binder increased tendency to intergranular failure. The formation of NbC and NbC0.84 phases after sintering was identified, indicating that some of the matrix carbon may have undergone graphitization. •Niobium at different concentrations was introduced as a binder for the PCD.•High integrity samples were prepared via HPHT route.•NbC and NbC0.84 phase formation was observed at diamond interfaces after sintering.•Metallic matrix increased young's modulus and tendency to intergranular failure.
ISSN:0263-4368
2213-3917
DOI:10.1016/j.ijrmhm.2020.105234