Effect of substrate surface roughness on properties of cold-sprayed copper coatings on SS316L steel
The development of thick pure copper coatings on SS316 substrates with desired properties for Tokamaks is still a challenging task. The solution to this task can help to fulfill the demanding requirements of in-vessel materials for plasma passivation. In the present work, the effect of substrate sur...
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Veröffentlicht in: | Surface & coatings technology 2020-05, Vol.389, p.125619, Article 125619 |
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Sprache: | eng |
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Zusammenfassung: | The development of thick pure copper coatings on SS316 substrates with desired properties for Tokamaks is still a challenging task. The solution to this task can help to fulfill the demanding requirements of in-vessel materials for plasma passivation. In the present work, the effect of substrate surface roughness on several properties of cold-sprayed copper coatings was investigated. Effect of post-heat-treatment on the properties of the developed coatings was also studied. The developed coatings were characterized using various techniques viz.; scanning electron microscopy/energy dispersive spectroscopy, X-ray diffraction, optical microscopy, microhardness, nanoindentation, electrical and thermal conductivity measurements, and density and porosity analyses. The novelty of the article includes in-situ micro-tensile testing of the developed coatings to understand their fracture mechanism, which showed multi-crack failure. Moreover, the cracks were found to be originating from the multi-splat boundary junctions, followed by growth along the splat boundaries. Additionally, γ-rays and heavy-nuclei irradiation along with thermal cyclic exposure studies were also performed to elucidate the actual environmental performance of the coatings. The coatings developed on the mirror-finished surface were found to have better mechanical and physical properties as compared to the coatings developed on the rough substrate surface; prior as-well-as post-heat-treatment.
•Substrate surface roughness influences coating properties in the vicinity of coating-substrate interface.•Mirror-finished substrate is suitable to achieve a better adhesion of cold sprayed copper coatings for Tokamak applications.•Heat-treatment of the cold-sprayed coatings resulted in a refined microstructure.•In-situ micro-tensile testing revealed the fracture behavior of cold-sprayed coatings. |
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ISSN: | 0257-8972 1879-3347 |
DOI: | 10.1016/j.surfcoat.2020.125619 |